ASTM D3174-12(2018)e1 - 15.10.2018
 
Significance and Use

5.1 Ash, as determined by this test method, is the residue remaining after burning the coal and coke. Ash obtained differs in composition from the inorganic constituents present in the original coal. Incineration causes an expulsion of all water, the loss of carbon dioxide from carbonates, the conversion of iron pyrites into ferric oxide, and other chemical reactions. Ash, as determined by this test method, will differ in amount from ash produced in furnace operations and other firing systems because incineration conditions influence the chemistry and amount of the ash. References for correcting ash results determined by this test method to a mineral-matter-free basis are listed in Classification D388, Section 9.

 
1. Scope

1.1 This test method covers the determination of the inorganic residue as ash in the analysis sample of coal or coke as prepared in accordance with Practice D2013 or Practice D346. The results obtained can be applied as the ash in the proximate analysis, Practice D3172, and in the ultimate analysis, Practice D3176. For the determination of the constituents in ash, reference is made to Test Methods D3682, D4326, and D6349. Test Methods D6357 should be used to prepare ash to be used for trace element analysis. See Terminology D121 for definition of ash.

1.2 The values stated in SI units are to be regarded as standard. The values given in parentheses after SI units are provided for information only and are not considered standard.

1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.

1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

 
2. Referenced Documents

D346-04

Standard Practice for Collection and Preparation of Coke Samples for Laboratory Analysis

D1757-03

Standard Test Method for Sulfate Sulfur in Ash from Coal and Coke (Withdrawn 2009)

D2795-95

Standard Test Methods for Analysis of Coal and Coke Ash (Withdrawn 2001)

D5016-16

Standard Test Method for Total Sulfur in Coal and Coke Combustion Residues Using a High-Temperature Tube Furnace Combustion Method with Infrared Absorption

D6349-21

Standard Test Method for Determination of Major and Minor Elements in Coal, Coke, and Solid Residues from Combustion of Coal and Coke by Inductively Coupled Plasma—Atomic Emission Spectrometry

D6357-21b

Standard Test Methods for Determination of Trace Elements in Coal, Coke, and Combustion Residues from Coal Utilization Processes by Inductively Coupled Plasma Atomic Emission Spectrometry, Inductively Coupled Plasma Mass Spectrometry, and Graphite Furnace Atomic Absorption Spectrometry (Includes all amendments and changes 12/17/2021).

E691-23

Standard Practice for Conducting an Interlaboratory Study to Determine the Precision of a Test Method

D388-23

Standard Classification of Coals by Rank

D2013-07

Standard Practice for Preparing Coal Samples for Analysis

D3172-13(2021)e1

Standard Practice for Proximate Analysis of Coal and Coke (Includes all amendments and changes 5/19/2021).

D3173-11

Standard Test Method for Moisture in the Analysis Sample of Coal and Coke

D3176-15(2023)

Standard Practice for Ultimate Analysis of Coal and Coke

D3180-15(2023)

Standard Practice for Calculating Coal and Coke Analyses from As-Determined to Different Bases

D3682-21

Standard Test Method for Major and Minor Elements in Combustion Residues from Coal Utilization Processes by Atomic Spectrometry

D4326-21

Standard Test Method for Major and Minor Elements in Coal Ash By X-Ray Fluorescence

D121-15(2024)

Standard Terminology of Coal and Coke