ASTM D4326-21 - 1.9.2021
 
Significance and Use

5.1?A compositional analysis of ash is used in describing the quality of coal for its complete characterization. Ash composition is useful in predicting slagging and fouling characteristics of combusted materials as well as the potential utilization of ash by-products.

5.2?The chemical composition of laboratory prepared coal ash is rarely, if ever, representative of the composition of the mineral matter in the coal because the ashing process can alter some minerals. However, it can approximate the composition of the fly ash and slag resulting from commercial combustion of coal.

 
1. Scope

1.1?This test method covers the analysis of the commonly determined major and minor elements in ash from coal using X-ray fluorescence (XRF) techniques.

Note 1:?Test Method D5016 is used for determination of sulfur.

Note 2:?Although not included in the present method, the determination of barium, strontium, and manganese may be required to yield adequate totals.

1.2?UnitsThe values stated in SI units are to be regarded as standard. The values given in parentheses after SI units are provided for information only and are not considered standard.

1.3?This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.

1.4?This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

 
2. Referenced Documents

D346-25

Standard Practice for Collection and Preparation of Coke Samples for Laboratory Analysis

D2013-07

Standard Practice for Preparing Coal Samples for Analysis

D3173-11

Standard Test Method for Moisture in the Analysis Sample of Coal and Coke

D3174-12(2018)e1

Standard Test Method for Ash in the Analysis Sample of Coal and Coke from Coal (Includes all amendments and changes 9/17/2020).

D5016-24

Standard Test Method for Total Sulfur in Coal and Coke Combustion Residues Using a High-Temperature Tube Furnace Combustion Method with Infrared Absorption

D7348-21

Standard Test Methods for Loss on Ignition (LOI) of Solid Combustion Residues

D7582-24

Standard Test Methods for Proximate Analysis of Coal and Coke by Macro Thermogravimetric Analysis

E2

Bulletin E2, Bulletin on Management of Naturally Occurring Radioactive Materials (NORM) in Oil and Gas Production, Second Edition

E11-24

Standard Specification for Woven Wire Test Sieve Cloth and Test Sieves

D121-24

Standard Terminology of Coal and Coke