ASTM D4377-00(2011) - 1.6.2011
 
Significance and Use

A knowledge of the water content of crude oil is important in the refining, purchase, sale, or transfer of crude oils.

 
1. Scope

1.1 This test method covers the determination of water in the range from 0.02 to 2 % in crude oils. Mercaptan and sulfide (S or H2S) sulfur are known to interfere with this test method (see Section 5).

1.2 This test method is intended for use with standard Karl Fischer reagent or pyridine-free Karl Fischer reagents.

1.3 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.

1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. Specific precautionary statements are given in Section 7.

 
2. Referenced Documents

E203-24

Standard Test Method for Water Using Volumetric Karl Fischer Titration

D4177-22e1

Standard Practice for Automatic Sampling of Petroleum and Petroleum Products (Includes all amendments and changes 3/24/2023).

D4057-22

Standard Practice for Manual Sampling of Petroleum and Petroleum Products

D4006-22

Standard Test Method for Water in Crude Oil by Distillation

D1193-24

Standard Specification for Reagent Water

MPMS Chapter 10.2

Determination of Water in Crude Oil by Distillation (ASTM Test Method )