ASTM D4493-20 - 1.6.2020
 
Significance and Use

5.1The solidification point of bisphenol A is a direct indication of its purity, although it gives no information as to the nature of any impurities present.

5.2High purity bisphenol A has a solidification point of approximately 157C.

5.3This test method can be used for internal quality control or for setting specifications.

 
1. Scope

1.1This test method describes the procedure for determination of the solidification point of bisphenol A (4,4'-isopropylidene diphenol).

1.2The test method has been found applicable for determination of the solidification point between 150 and 157C.

1.3In determining conformance of the test results using this method to applicable specifications, results shall be rounded off in accordance with the rounding-off method of Practice E29.

1.4The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.

1.5WarningMercury has been designated by many regulatory agencies as a hazardous substance that can cause serious medical issues. Mercury, or its vapor, has been demonstrated to be hazardous to health and corrosive to materials. Use caution when handling mercury and mercury-containing products. See the applicable product Safety Data Sheet (SDS) for additional information. The potential exists that selling mercury or mercury-containing products, or both, is prohibited by local or national law. Users must determine legality of sales in their location.

1.6This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. For specific hazard statements, see Section 9.

1.7This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

 
2. Referenced Documents

E1-14(2025)

Standard Specification for ASTM Liquid-in-Glass Thermometers

E29-22

Standard Practice for Using Significant Digits in Test Data to Determine Conformance with Specifications

D1493-97

Standard Test Method for Solidification Point of Industrial Organic Chemicals (Withdrawn 2004)

D4297-15(2024)

Standard Practice for Sampling and Handling Bisphenol A(4,4ยด -Isopropylidinediphenol)

D6809-24

Standard Guide for Quality Control and Quality Assurance Procedures for Aromatic Hydrocarbons and Related Materials

E691-23

Standard Practice for Conducting an Interlaboratory Study to Determine the Precision of a Test Method

E77-14(2021)

Standard Test Method for Inspection and Verification of Thermometers