ASTM D4821-01 - 10.12.2001
 
1. Scope

1.1 This guide covers a procedure for using ASTM Standard Reference Blacks (SRBs) to continuously monitor the precision of those carbon black test methods for which standard values have been established. It also offers guidelines for trouble-shooting various test methods.

1.2 This guide establishes the limits within which the statistical calibration procedure of Practice D3324 shall be applied and establishes the limits for an out-of-calibration condition beyond which the statistical calibration procedure of Practice D3324 shall not be applied.

1.3 This guide uses statistical control chart methodology as discussed in STP-15-D to determine if a laboratory's test results differ significantly from the accepted values of the SRBs and provides a format for reporting test data for specified tests on the SRB blacks.

1.4 The values stated in SI units are to be regarded as the standard. The values given in parentheses are for information only.

1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

 
2. Referenced Documents

D3493-26

Standard Test Method for Carbon Black—Oil Absorption Number of Compressed Sample (COAN)

D1510-25

Standard Test Method for Carbon Black—Iodine Adsorption Number

D1513-05(2023)

Standard Test Method for Carbon Black, Pelleted—Pour Density

D1765-23b

Standard Classification System for Carbon Blacks Used in Rubber Products (Includes all amendments and changes 1/29/2024).

D2414-26

Standard Test Method for Carbon Black—Oil Absorption Number (OAN)

D3324-01a

Standard Practice for Carbon Black—Improving Test Reproducibility Using ASTM Standard Reference Blacks (Withdrawn 2002)

D3265-24a

Standard Test Method for Carbon Black—Tint Strength (Includes all amendments and changes 7/16/2024).

E2586-19(2024)

Standard Practice for Calculating and Using Basic Statistics

E2282-23

Standard Guide for Defining the Test Result of a Test Method

E177-26a

Standard Practice for Use of the Terms Precision and Bias in ASTM Test Methods (Includes all amendments and changes 5/14/2026).

D6556-21

Standard Test Method for Carbon Black—Total and External Surface Area by Nitrogen Adsorption