ASTM D5060-12(2021)e1 - 1.1.2021
 
Significance and Use

4.1The test is suitable for setting specifications on ethylbenzene and for use as an internal quality control tool where ethylbenzene is used in manufacturing processes. It may be used in development or research work involving ethylbenzene.

4.2Purity is commonly reported by subtracting the determined expected impurities from 100 %. Absolute purity cannot be determined if unknown impurities are present.

 
1. Scope

1.1This test method describes the analysis of normally occurring impurities in, and the purity of, ethylbenzene by gas chromatography. Impurities determined include nonaromatic hydrocarbons, benzene, toluene, xylenes, cumene, and diethylbenzene isomers.

1.2This test method is applicable for impurities at concentrations from 0.001 to 1.000 % and for ethylbenzene purities of 99 % or higher. At this level, p-xylene may not be detected.

1.3In determining the performance of the test results using this method to applicable specifications, results shall be rounded off in accordance with the rounding-off method of Practice E29.

1.4The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.

1.5This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. For a specific hazard statement, see Section 8.

1.6This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

 
2. Referenced Documents

D6809-24

Standard Guide for Quality Control and Quality Assurance Procedures for Aromatic Hydrocarbons and Related Materials

E355-96(2021)e1

Standard Practice for Gas Chromatography Terms and Relationships (Includes all amendments and changes 4/28/2021).

E29-22

Standard Practice for Using Significant Digits in Test Data to Determine Conformance with Specifications

E1510-95(2021)

Standard Practice for Installing Fused Silica Open Tubular Capillary Columns in Gas Chromatographs

D4307-17(2021)

Standard Practice for Preparation of Liquid Blends for Use as Analytical Standards

D3437-15(2022)

Standard Practice for Sampling and Handling Liquid Cyclic Products