ASTM D5241-92(1998) - 10.7.1998
 
1. Scope

1.1 This practice covers standard procedures for extraction of volatile and semi-volatile organic compounds from water using small volumes of solvents.

1.2 The compounds of interest must have a greater solubility in the organic solvent than the water phase.

1.3 Not all of the solvents that can be used in micro extraction are addressed in this practice. The applicability of a solvent to extract the compound(s) of interest must be demonstrated before use.

1.4 This practice provides sample extracts suitable for any technique amenable to solvent injection such as gas chromatography or high performance liquid chromatography (HPLC).

1.5 The values stated in SI units are to be regarded as the standard.

1.6 This standard does not purport to address all of the safety problems, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. For specific hazard statements, see Section 9.

 
2. Referenced Documents

D1193-24

Standard Specification for Reagent Water

D3370-25

Standard Practices for Sampling Water from Flowing Process Streams

D1129-24

Standard Terminology Relating to Water

D5175-91(2024)

Standard Test Method for Organohalide Pesticides and Polychlorinated Biphenyls in Water by Microextraction and Gas Chromatography

D4448-01(2019)

Standard Guide for Sampling Ground-Water Monitoring Wells

D4210-89(1996)e1

Standard Practice for Intralaboratory Quality Control Procedures and a Discussion on Reporting Low-Level Data (Withdrawn 2002)

D3973-85(2024)

Standard Test Method for Low-Molecular Weight Halogenated Hydrocarbons in Water

D3856-11

Standard Guide for Management Systems in Laboratories Engaged in Analysis of Water

D3694-96(2024)

Standard Practices for Preparation of Sample Containers and for Preservation of Organic Constituents