ASTM D5297-95(2009) - 1.7.2009
 
Significance and Use

These test methods are designed to determine the purity of rubber chemical accelerators.

Since the results of these test methods are based on an integrated peak area, it is assumed that all analytes of interest are resolved from interfering peaks.

 
1. Scope

1.1 These test methods cover the determination of the purity of present commercially available rubber chemical accelerators in the range from 80 to 100 % by high performance liquid chromatography (HPLC) using ultraviolet detection and external standard calculations.

1.2 Expertise in HPLC is necessary to the successful application of these test methods.

1.3 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.

1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

 
2. Referenced Documents

D4571-22

Standard Test Methods for Rubber Compounding Materials—Determination of Volatile Material

D4936-10(2023)

Standard Test Method for Mercaptobenzothiazole Sulfenamide Assay by Reduction/Titration

D3853-22

Standard Terminology Relating to Rubber and Rubber Latices—Abbreviations for Chemicals Used in Compounding

ISO 6472

Rubber Compounding Ingredients--Abbreviations

D4483-25

Standard Practice for Evaluating Precision for Test Method Standards in the Rubber and Carbon Black Manufacturing Industries