ASTM D5368-93 - 1.1.2001
 
1. Scope

1.1 These test methods describe standard procedures for gravimetrically determining the total nonvolatile and semi-volatile organic content of solvent extracts from soils or solid wastes. The following methods are included:

Section
Method A--Micro-Determination of TSEC11-13
Method B--Evaporating Dish Procedure14-16
Method C--Boiling Flask Procedure17-19

1.2 These methods are used after a solvent extract is obtained from a soil or solid waste. For these methods to be applicable, the extraction solvent must have a boiling point less than that of water at ambient pressure.

1.3 The total solvent extractable content (TSEC) of a soil, sediment, sludge, or solid waste depends upon the solvent and method used for the extraction procedure.

 
2. Referenced Documents

D3694-96(2024)

Standard Practices for Preparation of Sample Containers and for Preservation of Organic Constituents

D3445-

Method of Test for Nonvolatile Matter in Trichlorotribluoroethane (Withdrawn 1991)

D3086-85

Test Method for Organochlorine Pesticides in Water (Withdrawn 1996)

D4281-95(2001)

Standard Test Method for Oil and Grease (Fluorocarbon Extractable Substances) by Gravimetric Determination

D2910-85

Method for Removal of Organic Matter from Water by Activated Carbon Absorption (Withdrawn 1991)

D2109-01(2022)

Standard Test Methods for Nonvolatile Matter in Halogenated Organic Solvents and Their Admixtures

D5369-93(1998)

Standard Practice for Extraction of Solid Waste Samples for Chemical Analysis Using Soxhlet Extraction

D5681-23

Standard Terminology for Waste and Waste Management