ASTM D5661-95(2001) - 1.1.2001
 
Significance and Use

PKP values indicate high aromatic or high naphthenic content, or both, which contributes to high relative solvency of the oil.

 
1. Scope

1.1 This test method covers a procedure for determining the relative solvency of petroleum oils used in ink formulations by a pentaerythritol ester of resin acids (PKP) titration.

1.2 This test method is applicable to petroleum oils that have an initial boiling point over 90oC and a dry point under 500oC as determined by Method D86.

1.3 This test method, along with viscosity measurements as determined by Test Method D445, is used to ensure the compositional consistency of petroleum oils. It can also differentiate between hydrotreated and non-hydrotreated oils that have the same viscosity.

1.4 This test method includes the use of a U.S. Occupational Safety and Health Administration (OSHA)-designated flammable chemical, pentane. Consult the suppliers' material safety data sheet for specific hazard information and guidance relative to use.

1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. Specific hazard statements are given in 1.3.

 
2. Referenced Documents

D445-26

Standard Test Method for Kinematic Viscosity of Transparent and Opaque Liquids (and Calculation of Dynamic Viscosity)

D86-23ae2

Standard Test Method for Distillation of Petroleum Products and Liquid Fuels at Atmospheric Pressure (Includes all amendments and changes 11/4/2024).

E691-23

Standard Practice for Conducting an Interlaboratory Study to Determine the Precision of a Test Method

D841-24

Standard Specification for Nitration Grade Toluene

D611-23

Standard Test Methods for Aniline Point and Mixed Aniline Point of Petroleum Products and Hydrocarbon Solvents