ASTM D5758-01(2011)e1 - 1.10.2011
 
1. Scope

1.1 This test method covers a procedure for determination of the relative crystallinity of zeolite ZSM-5 using selected peaks from the X-ray diffraction pattern of the zeolite.

1.2 The test method provides a number that is the ratio of intensity of a portion of the XRD pattern of the sample ZSM-5 to intensity of the corresponding portion of the pattern of a reference ZSM-5. The intensity ratio, expressed as a percentage, is then labeled percent XRD relative crystallinity/ZSM-5. This type of comparison is commonly used in zeolite technology and is often referred to as percent crystallinity.

1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

 
2. Referenced Documents

E456-13a(2022)e1

Standard Terminology Relating to Quality and Statistics (Includes all amendments and changes 4/16/2024).

E691-23

Standard Practice for Conducting an Interlaboratory Study to Determine the Precision of a Test Method

D3906-25

Standard Test Method for Determination of Relative X-ray Diffraction Intensities of Faujasite-Type Zeolite-Containing Materials

D5357-25

Standard Test Method for Determination of Relative Crystallinity of Zeolite Sodium A by X-ray Diffraction

E177-26a

Standard Practice for Use of the Terms Precision and Bias in ASTM Test Methods (Includes all amendments and changes 5/14/2026).