ASTM D5800-08 - 1.5.2008
 
Significance and Use

The evaporation loss is of particular importance in engine lubrication. Where high temperatures occur, portions of an oil can evaporate.

Evaporation may contribute to oil consumption in an engine and can lead to a change in the properties of an oil.

Many engine manufacturers specify a maximum allowable evaporation loss.

Some engine manufacturers, when specifying a maximum allowable evaporation loss, quote this test method along with the specifications.

Procedure C, using the Selby-Noack apparatus, also permits collection of the volatile oil vapors for determination of their physical and chemical properties. Elemental analysis of the collected volatiles may be helpful in identifying components such as phosphorous, which has been linked to premature degradation of the emission system catalyst.

 
1. Scope

1.1 This test method covers three procedures for determining the evaporation loss of lubricating oils (particularly engine oils). Procedure A uses the Noack evaporative tester equipment; Procedure B uses the automated non-Woods metal Noack evaporative apparatus; and Procedure C uses Selby-Noack volatility test equipment. The test method relates to one set of operating conditions but may be readily adapted to other conditions when required.

1.2 Noack results determined using Procedures A and B show consistent differences. Procedure A gives slightly lower results versus Procedure B on formulated engine oils, while Procedure A gives higher results versus Procedure B on basestocks.

1.3 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.

1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

 
2. Referenced Documents

D4177-22e1

Standard Practice for Automatic Sampling of Petroleum and Petroleum Products (Includes all amendments and changes 3/24/2023).

D6299-26a

Standard Practice for Applying Statistical Quality Assurance and Control Charting Techniques to Evaluate Analytical Measurement System Performance (Includes all amendments and changes 8/4/2026).

D6300-26

Standard Practice for Determination of Precision and Bias Data for Use in Test Methods for Petroleum Products, Liquid Fuels, and Lubricants

DIN 1725

Specification for Aluminum Alloys

DIN 12785

D4057-22

Standard Practice for Manual Sampling of Petroleum and Petroleum Products