ASTM D6201-19 - 1.11.2019
 
Significance and Use

5.1 Test Method—The Coordinating Research Council sponsored testing to develop this test method to evaluate a fuel's tendency to form intake valve deposits.

5.1.1 State and Federal Legislative and Regulatory Action—Regulatory action by California Air Resources Board (CARB)9 and the United States Environmental Protection Agency (EPA)10 necessitate the acceptance of a standardized test method to evaluate the intake system deposit forming tendency of an automotive spark-ignition engine fuel.

5.1.2 Relevance of Results—The operating conditions and design of the engine used in this test method are not representative of all engines. These factors shall be considered when interpreting test results.

5.2 Test Validity: 

5.2.1 Procedural Compliance—The test results are not considered valid unless the test is completed in compliance with all requirements of this test method. Deviations from the parameter limits presented in Sections 12 – 14 will result in an invalid test. Apply engineering judgment during conduct of the test method when assessing any anomalies to ensure validity of the test results.

5.2.2 Engine Compliance—A test is not considered valid unless the test engine meets the quality control inspection requirements as described in Sections 10 and 12.

 
1. Scope

1.1 This test method covers an engine dynamometer test procedure for evaluation of intake valve deposit formation of unleaded spark-ignition engine fuels.2 This test method uses a Ford Ranger 2.3 L four-cylinder engine. This test method includes detailed information regarding the procedure, hardware, and operations.

1.2 The ASTM Test Monitoring Center (TMC)3 is responsible for engine test stand calibration as well as issuance of information letters after test method modifications are approved by Subcommittee D02.A0 and Committee D02. Users of this test method shall request copies of recent information letters from the TMC to ensure proper conduct of the test method.

1.3 The values stated in SI units are to be regarded as standard. The values given in parentheses after SI units are provided for information only and are not considered standard.

1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. Specific warning statements are given throughout this test method.

1.5 This test method is arranged as follows:

Subject

Section

Scope

1

Referenced Documents

2

Terminology

3

Summary of Test Method

4

Significance and Use

5

Apparatus

6

 Laboratory Facilities

6.1

 Engine and Cylinder Head Build-Up and Measurement Area

6.1.1

 Engine Operating Area

6.1.2

 Fuel Injector Testing Area

6.1.3

 Intake Valve Rinsing and Parts Cleaning Area

6.1.4

 Parts Rating and Intake Valve Weighing Area

6.1.5

 Test Stand Laboratory Equipment

6.2

 Test Stand Configuration

6.2.1

 Dynamometer Speed and Load Control System

6.2.2

 Intake Air Supply System

6.2.3

 Exhaust System

6.2.4

 Fuel Supply System

6.2.5

 Engine Control Calibration

6.2.6

 Ignition System

6.2.7

 Engine Coolant System

6.2.8

 External Oil System

6.2.9

 Temperature Measurement Equipment and Locations

6.2.10

 Pressure Measurement Equipment and Locations

6.2.11

 Flow Measurement Equipment and Locations

6.2.12

 Speed and Load Measurement Equipment and Locations

6.2.13

 Exhaust Emissions Measurement Equipment and Location

6.2.14

 DPFE (EGR) Voltage Measurement Equipment and Location

6.2.15

 Ignition Timing Measurement Equipment and Location

6.2.16

 Test Engine Hardware

6.3

 Test Engine Parts

6.3.1

 New Parts Required

6.3.2

 Reusable Engine Parts

6.3.3

 Special Measurement and Assembly Equipment

6.4

Reagents and Materials

7

Hazards

8

Reference Fuel

9

Preparation of Apparatus

10

 Test Stand Preparation

10.1

 Engine Block Preparation

10.2

 Preparation of Miscellaneous Engine Components

10.3

 Cylinder Head Preparation

10.4

 Cylinder Head Assembly

10.5

 Cylinder Head Installation

10.6

 Final Engine Assembly

10.7

Calibration

11

 Test Stand Calibration

11.1

 Instrumentation Calibration

11.2

Procedure

12

 Pretest Procedure

12.1

 Engine Operating Procedure

12.2

 Periodic Measurements and Functions

12.3

 End of Test Procedures

12.4

Determination of Test Results

13

 Post-Test Intake Valve Weighing Procedure

13.1

 Photographs of Parts—General

13.2

 Induction System Rating

13.3

 Determination of Test Validity-Engine Conformance

13.4

Report

14

Precision and Bias

15

Keywords

16

Annexes

 

Detailed Specifications and Photographs of Apparatus

Annex A1

Engine Part Number Listing

Annex A2

Statistical Equations for Mean and Standard Deviation

Annex A3

1.6 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

 
2. Referenced Documents

D86-23ae2

Standard Test Method for Distillation of Petroleum Products and Liquid Fuels at Atmospheric Pressure (Includes all amendments and changes 11/4/2024).

D235-22

Standard Specification for Mineral Spirits (Petroleum Spirits) (Hydrocarbon Dry Cleaning Solvent)

D287-22

Standard Test Method for API Gravity of Crude Petroleum and Petroleum Products (Hydrometer/Method)

D381-25

Standard Test Method for Gum Content in Fuels by Jet Evaporation

D525-12a(2025)

Standard Test Method for Oxidation Stability of Gasoline (Induction Period Method) (Includes all amendments and changes 12/24/2025).

D873-22

Standard Test Method for Oxidation Stability of Aviation Fuels (Potential Residue Method)

D1266-18

Standard Test Method for Sulfur in Petroleum Products (Lamp Method) (Withdrawn 2025)

D1298-24

Standard Test Method for Density, Relative Density, or API Gravity of Crude Petroleum and Liquid Petroleum Products by Hydrometer Method

D1319-26

Standard Test Method for Hydrocarbon Types in Liquid Petroleum Products by Fluorescent Indicator Adsorption

J254

Instrumentation and Techniques for Exhaust Gas Emissions Measurement

D5302-01a

Test Method for Evaluation of Automotive Engine Oils for Inhibition of Deposit Formation and Wear in a Spark-Ignition Internal Combustion Engine Fueled with Gasoline and Operated Under Low-Temperature, Light-Duty Conditions (Withdrawn 2003)

D2427-06

Standard Test Method for Determination of C2 through C5 Hydrocarbons in Gasolines by Gas Chromatography

D2622-26

Standard Test Method for Sulfur in Petroleum Products by Wavelength Dispersive X-ray Fluorescence Spectrometry

E1064-24

Standard Test Method for Water in Organic Liquids by Coulometric Karl Fischer Titration

D5482-26

Standard Test Method for Vapor Pressure of Petroleum Products and Liquid Fuels (Mini Method—Atmospheric)

E203-24

Standard Test Method for Water Using Volumetric Karl Fischer Titration

MC96.1

Temperature Measurement-Thermocouples

CRC Manual 16,

Carburetor and Induction System Rating Manual

D1744-13

Standard Test Method for Determination of Water in Liquid Petroleum Products by Karl Fischer Reagent (Withdrawn 2016)

D3237-22

Standard Test Method for Lead in Gasoline by Atomic Absorption Spectroscopy

D4057-22

Standard Practice for Manual Sampling of Petroleum and Petroleum Products

D4294-24

Standard Test Method for Sulfur in Petroleum and Petroleum Products by Energy Dispersive X-ray Fluorescence Spectrometry

D4814-26

Standard Specification for Automotive Spark-Ignition Engine Fuel

D4953-26

Standard Test Method for Vapor Pressure of Gasoline and Gasoline-Oxygenate Blends (Dry Method)

D5059-26

Standard Test Methods for Lead and Manganese in Gasoline by X-Ray Fluorescence Spectroscopy

D5190-07

Standard Test Method for Vapor Pressure of Petroleum Products (Automatic Method) (Withdrawn 2012)

D5191-22

Standard Test Method for Vapor Pressure of Petroleum Products and Liquid Fuels (Mini Method)