ASTM D6750-10b - 1.10.2010
 
Significance and Use

These are accelerated engine oil tests (known as the 1K and 1N test procedures), performed in a standardized, calibrated, stationary single-cylinder diesel engine using either mass fraction 0.4 % sulfur fuel (1K test) or mass fraction 0.04 % sulfur fuel (1N test), that give a measure of (1) piston and ring groove deposit forming tendency, (2) piston, ring and liner scuffing and (3) oil consumption.

The 1K test was correlated with vehicles equipped with certain multi-cylinder direct injection engines used in heavy duty and high speed service prior to 1989, particularly with respect to aluminum piston deposits, and oil consumption, when fuel sulfur was nominally mass fraction 0.4 %. These data are given in Research Report RR:D02-1273.

The 1N test has been used to predict piston deposit formation in four-stroke cycle, direct injection, diesel engines that have been calibrated to meet 1994 U.S. federal exhaust emission requirements for heavy-duty engines operated on fuel containing less than mass fraction 0.05 % sulfur. See Research Report RR:D02-1321.

These test methods are used in the establishment of diesel engine oil specification requirements as cited in Specification D4485 for appropriate API Performance Category oils (API 1509).

These test methods are also used in diesel engine oil development.

 
1. Scope

1.1 These test methods cover the performance of engine oils intended for use in certain diesel engines. They are performed in a standardized high-speed, single-cylinder diesel engine by either the 1K (0.4 % mass fuel sulfur) or 1N (0.04 % mass fuel sulfur) procedure. The only difference in the two test methods is the fuel used. Piston and ring groove deposit-forming tendency and oil consumption are measured. Also, the piston, the rings, and the liner are examined for distress and the rings for mobility. These test methods are required to evaluate oils intended to satisfy API service categories CF-4 and CH-4 for 1K, and CG-4 for 1N of Specification D4485.

1.2 These test methods, although based on the original Caterpillar 1K/1N procedures, also embody TMC information letters issued before these test methods were first published. These test methods are subject to frequent change. Until the next revision of these test methods, TMC will update changes in these test methods by the issuance of information letters which shall be obtained from TMC (see Annex A15).

1.3 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.

1.3.1 ExceptionWhere there is no direct SI equivalent such as screw threads, national pipe threads/diameters, tubing size, or single source equipment specified. Also Brake Specific Fuel Consumption is measured in kilograms per kilowatthour.

1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. Specific precautionary statements appear throughout the text. Being engine tests, these test methods do have definite hazards that shall be met by safe practices (see Annex A16 on Safety Precautions).

 
2. Referenced Documents

D445-26

Standard Test Method for Kinematic Viscosity of Transparent and Opaque Liquids (and Calculation of Dynamic Viscosity)

D1298-24

Standard Test Method for Density, Relative Density, or API Gravity of Crude Petroleum and Liquid Petroleum Products by Hydrometer Method

D1319-25

Standard Test Method for Hydrocarbon Types in Liquid Petroleum Products by Fluorescent Indicator Adsorption

D2425-23

Standard Test Method for Hydrocarbon Types in Middle Distillates by Mass Spectrometry

D2500-23

Standard Test Method for Cloud Point of Petroleum Products and Liquid Fuels

D2622-26

Standard Test Method for Sulfur in Petroleum Products by Wavelength Dispersive X-ray Fluorescence Spectrometry

D2709-22

Standard Test Method for Water and Sediment in Middle Distillate Fuels by Centrifuge

SAE J183

Engine Oil Performance and Engine Service Classification Available from the Society of Automotive Engineers Inc., 400 Commonwealth Dr., Warrendale, PA 15096. Order SAE Handbook, Vol 3; the standard is not available separately.

API 1509

Engine Service Classification and Guide to Crankcase Oil Selection Available from the American Petroleum Institute, 1220 L St., NW, Washington, DC 20005.

ASTM Deposit Rating Manual 20

(Formerly CRC Manual 20) For Stock #TMCMNL20, visit the ASTM website, www.astm.org, or contact ASTM International Customer Service at service@astm.org.

D130-26

Standard Test Method for Corrosiveness to Copper from Petroleum Products by Copper Strip Test

D287-22

Standard Test Method for API Gravity of Crude Petroleum and Petroleum Products (Hydrometer/Method)

D482-25

Standard Test Method for Ash from Petroleum Products

D524-15(2025)e1

Standard Test Method for Ramsbottom Carbon Residue of Petroleum Products (Includes all amendments and changes 8/11/2025).

D613-26

Standard Test Method for Cetane Number of Diesel Fuel Oil

D664-24

Standard Test Method for Acid Number of Petroleum Products by Potentiometric Titration

D1796-22

Standard Test Method for Water and Sediment in Fuel Oils by the Centrifuge Method (Laboratory Procedure)

D3117-03

Standard Test Method for Wax Appearance Point of Distillate Fuels (Withdrawn 2010)

D4485-24

Standard Specification for Performance of Active API Service Category Engine Oils

D4737-21

Standard Test Method for Calculated Cetane Index by Four Variable Equation

D3524-14(2020)

Standard Test Method for Diesel Fuel Diluent in Used Diesel Engine Oils by Gas Chromatography

D4739-26

Standard Test Method for Base Number Determination by Potentiometric Hydrochloric Acid Titration

D5185-26

Standard Test Method for Multielement Determination of Used and Unused Lubricating Oils and Base Oils by Inductively Coupled Plasma Atomic Emission Spectrometry (ICP-AES)

D5862-09

Standard Test Method for Evaluation of Engine Oils in Two-Stroke Cycle Turbo-Supercharged 6V92TA Diesel Engine (Withdrawn 2009)

D6202-02

Standard Test Method for Automotive Engine Oils on the Fuel Economy of Passenger Cars and Light-Duty Trucks in the Sequence VIA Spark Ignition Engine (Withdrawn 2009)

D6594-26

Standard Test Method for Evaluation of Corrosiveness of Diesel Engine Oil at 135 °C

D7422-25

Standard Test Method for Evaluation of Diesel Engine Oils in T-12 Exhaust Gas Recirculation Diesel Engine

E29-22

Standard Practice for Using Significant Digits in Test Data to Determine Conformance with Specifications

IEEE/ASTM SI 10

Standard for Use of the International System of Units (SI): The Modern Metric System

D5186-24

Standard Test Method for Determination of the Aromatic Content and Polynuclear Aromatic Content of Diesel Fuels By Supercritical Fluid Chromatography

D5844-98

Standard Test Method for Evaluation of Automotive Engine Oils for Inhibition of Rusting (Sequence IID) (Withdrawn 2003)

D86-23ae2

Standard Test Method for Distillation of Petroleum Products and Liquid Fuels at Atmospheric Pressure (Includes all amendments and changes 11/4/2024).

D93-26

Standard Test Methods for Flash Point by Pensky-Martens Closed Cup Tester

D97-17b(2022)

Standard Test Method for Pour Point of Petroleum Products (Includes all amendments and changes 11/29/2022).

D235-22

Standard Specification for Mineral Spirits (Petroleum Spirits) (Hydrocarbon Dry Cleaning Solvent)