ASTM D6896-03 - 10.3.2003
 
1. Scope

1.1 This test method covers the measurement of the yield stress and viscosity of engine oils after cooling at controlled rates over a period of 43 or 45 h to a final test temperature of -20 or -25°C. The viscosity measurements are made at a shear stress of 525 Pa over a shear rate of 0.4 to 15 s-1. This test method is suitable for measurement of viscosities ranging from 4000 mPas to >400 000 mPa·s, and is suitable for yield stress measurements of 7 Pa to >350 Pa.

1.2 This test method is applicable for used diesel oils. The applicability and precision to other used or unused engine oils or to petroleum products other than engine oils has not been determined.

1.3 This test method uses the millipascal second (mPas) as the unit of viscosity. For information, the equivalent centipoise unit is shown in parentheses.

1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

 
2. Referenced Documents

ISO Guide 34

General Requirements for the Competence of Reference Material Producers

E563-22

Standard Practice for Preparation and Use of an Ice-Point Bath as a Reference Temperature

E644-11(2025)

Standard Test Methods for Testing Industrial Resistance Thermometers

E1137-97

Standard Specification for Industrial Platinum Resistance Thermometers

E2877-12(2019)

Standard Guide for Digital Contact Thermometers

ISO 17025

General Requirements for the Competence of Testing and Calibration Laboratories

D3829-20a

Standard Test Method for Predicting the Borderline Pumping Temperature of Engine Oil (Includes all amendments and changes 11/12/2020).

D4684-20a

Standard Test Method for Determination of Yield Stress and Apparent Viscosity of Engine Oils at Low Temperature (Includes all amendments and changes 11/17/2020).

D5133-20a

Standard Test Method for Low Temperature, Low Shear Rate, Viscosity/Temperature Dependence of Lubricating Oils Using a Temperature-Scanning Technique (Includes all amendments and changes 6/12/2020).