ASTM D7066-04(2017) - 1.9.2017
 
Significance and Use

5.1 The presence and concentration of oil and grease in domestic and industrial wastewater is of concern to the public because of its deleterious aesthetic effect and its impact on aquatic life.

5.2 Regulations and standards have been established that require monitoring of oil and grease in water and wastewater.

 
1. Scope

1.1 This test method covers the determination of oil and grease and nonpolar material in water and wastewater by an infrared (IR) determination of dimer/trimer of chlorotrifluoroethylene (S-316)2 extractable substances from an acidified sample. Included in this estimation of oil and grease are any other compounds soluble in the solvent.

1.2 This test method is applicable to measurement of the light fuel although loss of some light ends during extraction can be expected.

1.3 This test method defines oil and grease in water and wastewater as that which is extractable in the test method and measured by IR absorption at 2930 cm-1 or 3.4 microns. Similarly, this test method defines nonpolar material in water and wastewater as that oil and grease which is not adsorbed by silica gel in the test method and measured by IR absorption at 2930 cm-1.

1.4 This test method covers the range of 5 to 100 mg/L and may be extended to a lower or higher level by extraction of a larger or smaller sample volume collected separately.

1.5 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.

1.6 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine (Guide D3856) the applicability of regulatory limitations prior to use.

1.7 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

 
2. Referenced Documents

D1129-24

Standard Terminology Relating to Water

E178-21

Standard Practice for Dealing With Outlying Observations

E168-16(2023)

Standard Practices for General Techniques of Infrared Quantitative Analysis

D5847-22

Standard Practice for Writing Quality Control Specifications for Standard Test Methods for Water Analysis

D5810-96(2026)

Standard Guide for Spiking into Aqueous Samples

D2777-21

Standard Practice for Determination of Precision and Bias of Applicable Test Methods of Committee D19 on Water

D3856-11

Standard Guide for Management Systems in Laboratories Engaged in Analysis of Water

D3370-25

Standard Practices for Sampling Water from Flowing Process Streams

D1193-24

Standard Specification for Reagent Water