ASTM D887-82(2003)e1 - 29.10.1982
 
Significance and Use

The goal of sampling is to obtain for analysis a portion of the whole that is representative. The most critical factors are the selection of sampling areas and number of samples, the method used for sampling, and the maintenance of the integrity of the sample prior to analysis. Analysis of water-formed deposits should give valuable information concerning cycle system chemistry, component corrosion, erosion, the failure mechanism, the need for chemical cleaning, the method of chemical cleaning, localized cycle corrosion, boiler carryover, flow patterns in a turbine, and the rate of radiation build-up. Some sources of water-formed deposits are cycle corrosion products, make-up water contaminants, and condenser cooling water contaminants.

 
1. Scope

1.1 These practices cover the sampling of water-formed deposits for chemical, physical, biological, or radiological analysis. The practices cover both field and laboratory sampling. It also defines the various types of deposits. The following practices are included:

Sections
Practice A-Sampling Water-Formed Deposits From Tubing of Steam Generators and Heat Exchangers8 to 10
Practice B-Sampling Water-Formed Deposits From Steam Turbines 11 to 14

1.2 The general procedures of selection and removal of deposits given here can be applied to a variety of surfaces that are subject to water-formed deposits. However, the investigator must resort to his individual experience and judgment in applying these procedures to his specific problem.

1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. See Section 7, 9.8, 9.8.4.6, and 9.14 for specific hazards statements.

 
2. Referenced Documents

D3483-14(2022)

Standard Test Methods for Accumulated Deposition in a Steam Generator Tube

D2331-08(2022)

Standard Practices for Preparation and Preliminary Testing of Water-Formed Deposits

D1293-18

Standard Test Methods for pH of Water

D1245-17(2025)

Standard Practice for Examination of Water-Formed Deposits by Chemical Microscopy

D2332-13(2021)

Standard Practice for Analysis of Water-Formed Deposits by Wavelength-Dispersive X-Ray Fluorescence

D1129-24

Standard Terminology Relating to Water

D934-22

Standard Practices for Identification of Crystalline Compounds in Water-Formed Deposits By X-Ray Diffraction

D512-23

Standard Test Methods for Chloride Ion In Water

D4412-19(2024)

Standard Test Methods for Sulfate-Reducing Bacteria in Water and Water-Formed Deposits

D1193-24

Standard Specification for Reagent Water