ASTM E394-22 - 1.9.2022
 
Significance and Use

4.1?This test method is suitable for determining trace concentrations of iron in a wide variety of products, provided that appropriate sample preparation has rendered the iron and sample matrix soluble in water or other suitable solvent (see 10.1 and Note 4).

4.2?This test method assumes that the amount of color developed is proportional to the amount of iron in the test solution. The calibration curve is linear over the specified range. Possible interferences are described in Section 5.

 
1. Scope

1.1?This test method covers the determination of trace concentrations of iron in the range from 1 to 100 ?g/g in a wide variety of products.

1.2?In determining the conformance of the test results using this method to applicable specifications; results shall be rounded off in accordance with the rounding-off method of Practice E29.

1.3?The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.

1.4?Consult current OSHA regulations, suppliers Safety Data Sheets, and local regulations for all materials used in this specification.

1.5?This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

 
2. Referenced Documents

E275-08(2022)

Standard Practice for Describing and Measuring Performance of Ultraviolet and Visible Spectrophotometers

E200-23

Standard Practice for Preparation, Standardization, and Storage of Standard and Reagent Solutions for Chemical Analysis

E180-03

Standard Practice for Determining the Precision of ASTM Methods for Analysis and Testing of Industrial and Specialty Chemicals (Withdrawn 2009)

E60-11(2022)e1

Standard Practice for Analysis of Metals, Ores, and Related Materials by Spectrophotometry (Includes all amendments and changes 6/29/2022).

D1193-24

Standard Specification for Reagent Water