ASTM B689-97(2023) - 1.5.2023
 
1. Scope

1.1?This specification covers the requirements for electroplated nickel coatings applied to metal products for engineering applications, for example, for use as a buildup for mismachined or worn parts, for electronic applications, including as underplates in contacts or interconnections, and in certain joining applications.

1.2?Electroplating of nickel for engineering applications (Note 1) requires technical considerations significantly different from decorative applications because the following functional properties are important:

1.2.1?Hardness, strength, and ductility,

1.2.2?Wear resistance,

1.2.3?Load bearing characteristics,

1.2.4?Corrosion resistance,

1.2.5?Heat scaling resistance,

1.2.6?Fretting resistance, and

1.2.7?Fatigue resistance.

Note 1:?Functional electroplated nickel coatings usually contain about 99 % nickel, and are most frequently electrodeposited from a Watts nickel bath or a nickel sulfamate bath. Typical mechanical properties of nickel electroplated from these baths, and the combined effect of bath operation and solution composition variables on the mechanical properties of the electrodeposit are given in Guide B832. When electroplated nickel is required to have higher hardnesses, greater wear resistance, certain residual stress values and certain leveling characteristics, sulfur and other substances are incorporated in the nickel deposit through the use of certain addition agents in the electroplating solution. For the effect of such additives, see Section 4 and Annex A3. Cobalt salts are sometimes added to the plating solution to produce harder nickel alloy deposits.

1.3?This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.

1.4?This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

 
2. Referenced Documents

B253-11(2022)

Standard Guide for Preparation of Aluminum Alloys for Electroplating

B254-92(2020)e1

Standard Practice for Preparation of and Electroplating on Stainless Steel (Includes all amendments and changes 12/7/2020).

B343-92a(2020)

Standard Practice for Preparation of Nickel for Electroplating with Nickel (Includes all amendments and changes 12/4/2020).

B374-21

Standard Terminology Relating to Electroplating

B480-88(2022)

Standard Guide for Preparation of Magnesium and Magnesium Alloys for Electroplating

B487-20

Standard Test Method for Measurement of Metal and Oxide Coating Thickness by Microscopical Examination of Cross Section

B499-09(2021)e1

Standard Test Method for Measurement of Coating Thicknesses by the Magnetic Method: Nonmagnetic Coatings on Magnetic Basis Metals (Includes all amendments and changes 5/18/2021).

B507-14(2021)

Standard Practice for Design of Articles to Be Electroplated on Racks

B530-09(2021)

Standard Test Method for Measurement of Coating Thicknesses by the Magnetic Method: Electrodeposited Nickel Coatings on Magnetic and Nonmagnetic Substrates

B558-79(2019)

Standard Practice for Preparation of Nickel Alloys for Electroplating

B568-98(2021)

Standard Test Method for Measurement of Coating Thickness by X-Ray Spectrometry

B571-23

Standard Practice for Qualitative Adhesion Testing of Metallic Coatings

B320-60(2019)

Standard Practice for Preparation of Iron Castings for Electroplating

B697-88(2021)

Standard Guide for Selection of Sampling Plans for Inspection of Electrodeposited Metallic and Inorganic Coatings

B765-03(2023)

Standard Guide for Selection of Porosity and Gross Defect Tests for Electrodeposits and Related Metallic Coatings

B809-95(2018)

Standard Test Method for Porosity in Metallic Coatings by Humid Sulfur Vapor (“Flowers-of-Sulfur”)

B832-93(2023)

Standard Guide for Electroforming with Nickel and Copper

B849-02(2023)

Standard Specification for Pre-Treatments of Iron or Steel for Reducing Risk of Hydrogen Embrittlement

B322-99(2020)e1

Standard Guide for Cleaning Metals Prior to Electroplating (Includes all amendments and changes 12/7/2020).

D762-49

Method of Test for Hot Extraction of Asphaltic Materials and Recovery of Bitumen by the Modified Abson Procedure

D1193-06(2018)

Standard Specification for Reagent Water

D3951-18(2023)

Standard Practice for Commercial Packaging

F519-23

Standard Test Method for Mechanical Hydrogen Embrittlement Evaluation of Plating/Coating Processes and Service Environments

B850-98(2022)

Standard Guide for Post-Coating Treatments of Steel for Reducing the Risk of Hydrogen Embrittlement

B851-04(2020)

Standard Specification for Automated Controlled Shot Peening of Metallic Articles Prior to Nickel, Autocatalytic Nickel, or Chromium Plating, or as Final Finish

B281-88(2019)e1

Standard Practice for Preparation of Copper and Copper-Base Alloys for Electroplating and Conversion Coatings (Includes all amendments and changes 5/14/2019).

B602-21

Standard Guide for Attribute Sampling of Metallic and Inorganic Coatings

B183-18(2022)

Standard Practice for Preparation of Low-Carbon Steel for Electroplating

B242-99(2020)

Standard Guide for Preparation of High-Carbon Steel for Electroplating

B252-92(2020)

Standard Guide for Preparation of Zinc Alloy Die Castings for Electroplating and Conversion Coatings