ASTM B859-03 - 1.10.2003
 
1. Scope

1.1 This practice covers the de-agglomeration of refractory metal powders and their compounds in preparation for particle size analysis.

1.2 Experience has shown that this practice is satisfactory for the de-agglomeration of elemental tungsten, molybdenum, rhenium, and tantalum metal powders, and tungsten carbide. Other metal powders (for example, elemental metals, carbides, and nitrides) may be prepared for particle size analysis using this practice with caution as to effectiveness until actual satisfactory experience is developed.

1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. For specific precautionary statements, see Note 2.

 
2. Referenced Documents

B821-23

Standard Guide for Liquid Dispersion of Metal Powders and Related Compounds for Particle Size Analysis

B822-25

Standard Test Method for Particle Size Distribution of Metal Powders and Related Compounds by Light Scattering

Detailed Drawings of Alternative Steel Milling Bottles Available from ASTM International Headquarters. Order Adjunct No. .

B243-26a

Standard Terminology of Powder Metallurgy (Includes all amendments and changes 6/8/2026).

B761-26

Standard Test Method for Particle Size Distribution of Metal Powders and Related Compounds by X-Ray Monitoring of Gravity Sedimentation

B330-20(2024)e1

Standard Test Methods for Estimating Average Particle Size of Metal Powders and Related Compounds Using Air Permeability (Includes all amendments and changes 10/29/2024).