ASTM C1001-00 - 10.8.2000
 
1. Scope

1.1 This test method covers the determination of plutonium in soils at levels of detection dependent on count time, sample size, detector efficiency, background, and tracer yield. This test method describes one acceptable approach to the determination of plutonium in soil.

1.2 This test method is designed for 10 g of soil, previously collected and treated as described in Practices C998 and C999, but sample sizes up to 50 g may be analyzed by this test method. This test method may not be able to completely dissolve all forms of plutonium in the soil matrix.

1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. Specific hazard statements are given in Sections 6 and 9.

 
2. Referenced Documents

C999-26

Standard Practice for Soil Sample Preparation for the Determination of Radionuclides

C998-26

Standard Practice for Sampling Surface Soil for Radionuclides

C859-26

Standard Terminology Relating to Nuclear Materials

C1163-14(2023)

Standard Practice for Mounting Actinides for Alpha Spectrometry Using Neodymium Fluoride

D7282-24

Standard Practice for Setup, Calibration, and Quality Control of Instruments Used for Radioactivity Measurements

D3648-23

Standard Practices for the Measurement of Radioactivity

D3084-20

Standard Practice for Alpha-Particle Spectrometry of Water

C1284-18

Standard Practice for Electrodeposition of the Actinides for Alpha Spectrometry

D1193-24

Standard Specification for Reagent Water