ASTM C1022-05 - 1.1.2005
 
Significance and Use

The test methods in this standard are designed to show whether a given material meets the specifications prescribed in Specification C 967.

Because of the variability of matrices of uranium-ore concentrate and the lack of suitable reference or calibration materials, the precision and bias of these test methods should be established by each individual laboratory that will use them. The precision and bias statements given for each test method are those reported by various laboratories and can be used as a guideline.

Instrumental test methods such as X-ray fluorescence and emission spectroscopy can be used for the determination of some impurities where such equipment is available.

 
1. Scope

1.1 These test methods cover procedures for the chemical and atomic absorption analysis of uranium-ore concentrates to determine compliance with the requirements prescribed in Specification C 967.

1.2 The analytical procedures appear in the following order:

This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. A specific precautionary statement is given in Section 7.

 
2. Referenced Documents

C1110-03

Standard Practice for Sample Preparation for X-Ray Emission Spectrometric Analysis of Uranium in Ores Using the Glass Fusion or Pressed Powder Method

C1219-05

Standard Test Methods for Arsenic in Uranium Hexafluoride

C1254-26

Standard Test Method for Determination of Uranium in Mineral Acids by X-Ray Fluorescence

C1267-17(2022)

Standard Test Method for Uranium by Iron (II) Reduction in Phosphoric Acid Followed by Chromium (VI) Titration in the Presence of Vanadium

C1287-18

Standard Test Method for Determination of Impurities in Nuclear Grade Uranium Compounds by Inductively Coupled Plasma Mass Spectrometry

D1193-24

Standard Specification for Reagent Water

E60-11(2022)e1

Standard Practice for Analysis of Metals, Ores, and Related Materials by Spectrophotometry (Includes all amendments and changes 6/29/2022).

C1347-08(2023)

Standard Practice for Preparation and Dissolution of Uranium Materials for Analysis

C761-24

Standard Test Methods for Chemical, Mass Spectrometric, Spectrochemical, Nuclear, and Radiochemical Analysis of Uranium Hexafluoride

C859-26

Standard Terminology Relating to Nuclear Materials

C967-25

Standard Specification for Uranium Ore Concentrate