ASTM C1285-97 - 10.10.1997
 
1. Scope

1.1 These product consistency test methods A and B evaluate the chemical durability of homogeneous and devitrified glasses by measuring the concentrations of the chemical species released from a crushed glass to a test solution.

1.1.1 Test Method A is a seven-day crushed glass durability test performed at 90 + 2°C in a leachant of ASTM-Type I water. The test method is static and conducted in stainless steel vessels. Test Method A can specifically be used to evaluate whether the durability and elemental release characteristics of waste glasses have been consistently controlled during production. This test method is applicable to radioactive and simulated waste glasses.

1.1.2 Test Method B is a crushed glass durability test that allows testing of water glasses at varying test durations, test temperatures, ratios of glass surface area ( ) to leachant volume ( ), and leachant types. This test method is static and can be conducted in stainless steel or PFA TFE-fluorocarbon vessels, or both. Test Method B can specifically be used to evaluate the relative durability characteristics of homogeneous or devitrified glasses, or both. This test method is applicable to radioactive and simulated waste glasses. Test Method B cannot be used as a consistency test for production of high level radioactive waste glass.

1.2 These test methods must be performed in accordance with all quality assurance requirements for acceptance of the data.

1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

 
2. Referenced Documents

C1463-19

Standard Practices for Dissolving Glass Containing Radioactive and Mixed Waste for Chemical and Radiochemical Analysis

C1662-24e1

Standard Test Method for Measurement of the Dissolution Rate of Nuclear Waste Forms Using the Single-Pass Flow-Through Test Method (Includes all amendments and changes 7/16/2025).

D859-16(2021)e1

Standard Test Method for Silica in Water (Includes all amendments and changes 12/6/2021).

D1129-24

Standard Terminology Relating to Water

D1193-24

Standard Specification for Reagent Water

E177-26a

Standard Practice for Use of the Terms Precision and Bias in ASTM Test Methods (Includes all amendments and changes 5/14/2026).

E456-13a(2022)e1

Standard Terminology Relating to Quality and Statistics (Includes all amendments and changes 4/16/2024).

E1402-13(2023)

Standard Guide for Sampling Design

C1220-21

Standard Test Method for Static Leaching of Monolithic Waste Forms for Disposal of Radioactive Waste

D1293-18

Standard Test Methods for pH of Water

D4327-17(2025)

Standard Test Method for Anions in Water by Suppressed Ion Chromatography

D5956-21

Standard Guide for Sampling Strategies for Heterogeneous Wastes

E7-25

Standard Terminology Relating to Metallography

E691-23

Standard Practice for Conducting an Interlaboratory Study to Determine the Precision of a Test Method

C162-23

Standard Terminology of Glass and Glass Products

C429-21(2025)

Standard Test Method for Sieve Analysis of Raw Materials for Glass Manufacture

C693-24

Standard Test Method for Density of Glass by Buoyancy

C92-95(2022)e1

Standard Test Methods for Sieve Analysis and Water Content of Refractory Materials (Includes all amendments and changes 4/22/2022).

C169-16(2022)

Standard Test Methods for Chemical Analysis of Soda-Lime and Borosilicate Glass

C225-85(2022)

Standard Test Methods for Resistance of Glass Containers to Chemical Attack

C371-09(2024)

Standard Test Method for Wire-Cloth Sieve Analysis of Nonplastic Ceramic Powders

C859-26

Standard Terminology Relating to Nuclear Materials

C1109-23

Standard Practice for Analysis of Aqueous Leachates from Nuclear Waste Materials Using Inductively Coupled Plasma-Atomic Emission Spectroscopy

C1174-20

Standard Guide for Evaluation of Long-Term Behavior of Materials Used in Engineered Barrier Systems (EBS) for Geological Disposal of High-Level Radioactive Waste