5.1There are existing lime-based flue gas desulfurization units in operation that require a method to measure the oxides available for sulfur dioxide absorption. Dissolved magnesium oxide varies among limes depending on the limestone sources and calcination conditions.

1.1This test method covers analysis of magnesian, dolomitic and high-calcium limes for total neutralizing capability and dissolved major oxides. Dissolved calcium and magnesium are the major species that neutralize acid under the conditions of the test.

1.2The test conditions are chosen to measure the acid-neutralizing capacity of both calcium hydroxide and magnesium hydroxide contained in slaked lime. By controlling the neutralization pH at 6, magnesium hydroxide and magnesium oxide are titrated in addition to calcium hydroxide fraction.

1.3This test method also determines the fraction of Mg ions present in the lime that will dissolve under lime flue gas desulfurization (FGD) conditions. Because the Mg²⁺ ion alters FGD performance, it is important to know its concentration.

1.4The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.

1.5This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.

1.6This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.