ASTM C1470-20 - 1.1.2020
 
Significance and Use

5.1 The high-temperature capabilities of advanced ceramics are a key performance benefit for many demanding engineering applications. In many of those applications, advanced ceramics will have to perform across a broad temperature range. The thermal expansion, thermal diffusivity/conductivity, specific heat, and emittance/emissivity are crucial engineering factors in integrating ceramic components into aerospace, automotive, and industrial systems.

5.2 This guide is intended to serve as a reference and information source for testing the thermal properties of advanced ceramics, based on an understanding of the relationships between the composition and microstructure of these materials and their thermal properties.

5.3 The use of this guide assists the testing community in correctly applying the ASTM thermal test methods to advanced ceramics to ensure that the thermal test results are properly measured, interpreted, and understood. This guide also assists the user in selecting the appropriate thermal test method to evaluate the particular thermal properties of the advanced ceramic of interest.

5.4 The thermal properties of advanced ceramics are critical data in the development of ceramic components for aerospace, automotive, and industrial applications. In addition, the effect of environmental exposure on thermal properties of the advanced ceramics must also be assessed.

 
1. Scope

1.1 This guide covers the thermal property testing of advanced ceramics, to include monolithic ceramics, particulate/ whisker-reinforced ceramics, and continuous fiber-reinforced ceramic composites. It is intended to provide guidance and information to users on the special considerations involved in determining the thermal properties of these ceramic materials.

1.2 Five thermal properties (specific heat capacity, thermal conductivity, thermal diffusivity, thermal expansion, and emittance/emissivity) are presented in terms of their definitions and general test methods. The relationship between thermal properties and the composition, microstructure, and processing of advanced ceramics (monolithic and composite) is briefly outlined, providing guidance on which material and specimen characteristics have to be considered in evaluating the thermal properties of advanced ceramics. Additional sections describe sampling considerations, test specimen preparation, and reporting requirements.

1.3 Current ASTM test methods for thermal properties are tabulated in terms of test method concept, testing range, specimen requirements, standards/reference materials, capabilities, limitations, precision, and special instructions for monolithic and composite ceramics.

1.4 This guide is based on the use of current ASTM standards for thermal properties, where appropriate, and on the development of new test standards, where necessary. It is not the intent of this guide to rigidly specify particular thermal test methods for advanced ceramics. Guidance is provided on how to utilize the most commonly available ASTM thermal test methods, considering their capabilities and limitations.

1.5 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard. See IEEE/ASTM SI 10.

1.6 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.

1.7 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

 
2. Referenced Documents

C1045-19

Standard Practice for Calculating Thermal Transmission Properties Under Steady-State Conditions

IEEE/ASTM SI?10

Standard for Use of the International System of Units (SI) (The Modern Metric System)

E473-23b

Standard Terminology Relating to Thermal Analysis and Rheology (Includes all amendments and changes 10/5/2023).

E1142-23b

Standard Terminology Relating to Thermophysical Properties (Includes all amendments and changes 10/5/2023).

E122-17(2022)

Standard Practice for Calculating Sample Size to Estimate, With Specified Precision, the Average for a Characteristic of a Lot or Process

C372-94(2020)

Standard Test Method for Linear Thermal Expansion of Porcelain Enamel and Glaze Frits and Fired Ceramic Whiteware Products by Dilatometer Method

C351-92b(1999)

Standard Test Method for Mean Specific Heat of Thermal Insulation

E289-17

Standard Test Method for Linear Thermal Expansion of Rigid Solids with Interferometry

E831-19

Standard Test Method for Linear Thermal Expansion of Solid Materials by Thermomechanical Analysis

C714-23

Standard Guide for Thermal Diffusivity of Carbon and Graphite by Thermal Pulse Method

E1461-13(2022)

Standard Test Method for Thermal Diffusivity by the Flash Method

E408-13(2019)

Standard Test Methods for Total Normal Emittance of Surfaces Using Inspection-Meter Techniques

E423-71(2019)

Standard Test Method for Normal Spectral Emittance at Elevated Temperatures of Nonconducting Specimens

C373-18(2023)

Standard Test Methods for Determination of Water Absorption and Associated Properties by Vacuum Method for Pressed Ceramic Tiles and Glass Tiles and Boil Method for Extruded Ceramic Tiles and Non-tile Fired Ceramic Whiteware Products

C1145-19

Standard Terminology of Advanced Ceramics

C1300-95(2020)

Standard Test Method for Linear Thermal Expansion of Glaze Frits and Ceramic Whiteware Materials by Interferometric Method

E228-22

Standard Test Method for Linear Thermal Expansion of Solid Materials With a Push-Rod Dilatometer

D2766-95(2000)

Standard Test Method for Specific Heat of Liquids and Solids

E1269-11(2018)

Standard Test Method for Determining Specific Heat Capacity by Differential Scanning Calorimetry

C177-19e1

Standard Test Method for Steady-State Heat Flux Measurements and Thermal Transmission Properties by Means of the Guarded-Hot-Plate Apparatus (Includes all amendments and changes 2/23/2023).

C182-19

Standard Test Method for Thermal Conductivity of Insulating Firebrick

C201-93(2019)e1

Standard Test Method for Thermal Conductivity of Refractories (Includes all amendments and changes 11/2/2022).

C202-19

Standard Test Method for Thermal Conductivity of Refractory Brick

C408-88(2020)

Standard Test Method for Thermal Conductivity of Whiteware Ceramics

C518-21

Standard Test Method for Steady-State Thermal Transmission Properties by Means of the Heat Flow Meter Apparatus

C767-20

Standard Test Method for Thermal Conductivity of Carbon Refractories

C1044-16(2020)

Standard Practice for Using a Guarded-Hot-Plate Apparatus or Thin-Heater Apparatus in the Single-Sided Mode

C1045-19

Standard Practice for Calculating Thermal Transmission Properties Under Steady-State Conditions

C1113-99

Standard Test Method for Thermal Conductivity of Refractories by Hot Wire (Platinum Resistance Thermometer Technique)

C1114-06(2019)

Standard Test Method for Steady-State Thermal Transmission Properties by Means of the Thin-Heater Apparatus

C1130-21

Standard Practice for Calibration of Thin Heat Flux Transducers

E1225-20

Standard Test Method for Thermal Conductivity of Solids Using the Guarded-Comparative-Longitudinal Heat Flow Technique

E1530-19

Standard Test Method for Evaluating the Resistance to Thermal Transmission by the Guarded Heat Flow Meter Technique