ASTM C1502-01 - 10.6.2001
 
Significance and Use

The method is designed to show whether or not the tested materials meet the specifications as given in either Specification C 753, C 776, C 888 or C 922.

 
1. Scope

1.1 This test method covers the determination of chlorine and fluorine in nuclear-grade uranium dioxide (UO2) powder and pellets, nuclear grade gadolinium oxide (Gd2O3) powder and gadolinium oxide-uranium oxide (Gd2O3-UO2) powder and pellets.

1.2 With a 2 gram UO2 sample size the detection limit of the method is 4 μg/g for chlorine and 2 μg/g for fluorine. The maximum concentration determined with a 2 gram sample is 500 μg/g for both chlorine and fluorine. The sample size used in this test method can vary from 1 to 10 grams resulting in a corresponding change in the detection limits and range.

1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

 
2. Referenced Documents

C776-17(2022)

Standard Specification for Sintered Uranium Dioxide Pellets for Light Water Reactors

C859-26

Standard Terminology Relating to Nuclear Materials

C888-18(2026)

Standard Specification for Nuclear-Grade Gadolinium Oxide (Gd2O3) Powder

C922-21

Standard Specification for Sintered Gadolinium Oxide-Uranium Dioxide Pellets for Light Water Reactors

D1193-24

Standard Specification for Reagent Water

C753-16a(2021)

Standard Specification for Nuclear-Grade, Sinterable Uranium Dioxide Powder (Includes all amendments and changes 10/22/2021).