ASTM C289-03 - 10.8.2003
 
Significance and Use

When this test method is used to evaluate the potential reactivity of siliceous components in the aggregate with alkalies in hydraulic-cement concrete, it must be used in combination with other methods. Do not use the results of tests by this test method as the sole basis for acceptance or rejection for sources with regard to ASR.

Reactions between a sodium hydroxide solution and siliceous components in the aggregate have been shown to correlate with the performance of some aggregates in concrete structures. The results from this test method can be obtained quickly, and, while not completely reliable in all cases, they can provide useful data.

This test method can be employed as a quality control tool to periodically check samples from an existing source with an acceptable service history.

 
1. Scope

1.1 This test method covers chemical determination of the potential reactivity of an aggregate with alkalies in portland-cement concrete as indicated by the amount of reaction during 24 h at 80°C between 1 N sodium hydroxide solution and aggregate that has been crushed and sieved to pass a 300-μm sieve and be retained on a 150-μm sieve.

1.2 The values stated in SI units are to be regarded as standard.

1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. A specific precautionary statement is given in 5.7.1.

 
2. Referenced Documents

C295-08

Standard Guide for Petrographic Examination of Aggregates for Concrete

C114-24

Standard Test Methods for Chemical Analysis of Hydraulic Cement

C227-10

Standard Test Method for Potential Alkali Reactivity of Cement-Aggregate Combinations (Mortar-Bar Method) (Withdrawn 2018)

C1005-20

Standard Specification for Reference Masses and Devices for Determining Mass and Volume for Use in Physical Testing of Hydraulic Cements

D1248-25

Standard Specification for Polyethylene Plastics Extrusion Materials for Wire and Cable

C1260-23

Standard Test Method for Potential Alkali Reactivity of Aggregates (Mortar-Bar Method)

D1193-24

Standard Specification for Reagent Water

D75-03

Standard Practice for Sampling Aggregates

C1293-20

Standard Test Method for Determination of Length Change of Concrete Due to Alkali-Silica Reaction

E11-24

Standard Specification for Woven Wire Test Sieve Cloth and Test Sieves

C702-98

Standard Practice for Reducing Samples of Aggregate to Testing Size

Reagent Chemicals, American Chemical Society Specifications

E60-11(2022)e1

Standard Practice for Analysis of Metals, Ores, and Related Materials by Spectrophotometry (Includes all amendments and changes 6/29/2022).