ASTM D5184-22 - 1.10.2022
 
Significance and Use

5.1?Catalyst fines in fuel oils can cause abnormal engine wear. These test methods provide a means of determining silicon and aluminum, the major constituents of the catalysts.

 
1. Scope

1.1?These test methods cover the determination of aluminum and silicon in fuel oils at concentrations between 5 mg/kg and 150 mg/kg for aluminum and 10 mg/kg and 250 mg/kg for silicon.

1.2?Test Method AInductively coupled plasma atomic emission spectrometry is used in this test method to quantitatively determine aluminum and silicon.

1.3?Test Method BFlame atomic absorption spectrometry is used in this test method to quantitatively determine aluminum and silicon.

1.4?The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.

1.5?This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. Specific warning statements are given in Sections 7.6, 10.1, and 11.5.

1.6?This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

 
2. Referenced Documents

D4057-22

Standard Practice for Manual Sampling of Petroleum and Petroleum Products

E135-23a

Standard Terminology Relating to Analytical Chemistry for Metals, Ores, and Related Materials (Includes all amendments and changes 7/17/2023).

D7740-20

Standard Practice for Optimization, Calibration, and Validation of Atomic Absorption Spectrometry for Metal Analysis of Petroleum Products and Lubricants

D4177-22e1

Standard Practice for Automatic Sampling of Petroleum and Petroleum Products (Includes all amendments and changes 3/24/2023).

D1193-06(2018)

Standard Specification for Reagent Water

D6299-23a

Standard Practice for Applying Statistical Quality Assurance and Control Charting Techniques to Evaluate Analytical Measurement System Performance (Includes all amendments and changes 12/12/2023).

D6792-23c

Standard Practice for Quality Management Systems in Petroleum Products, Liquid Fuels, and Lubricants Testing Laboratories (Includes all amendments and changes 12/7/2023).

D7260-20

Standard Practice for Optimization, Calibration, and Validation of Inductively Coupled Plasma-Atomic Emission Spectrometry (ICP-AES) for Elemental Analysis of Petroleum Products and Lubricants