ASTM D4221-99 - 10.6.1999
 
1. Scope

1.1 This test method, when used in conjunction with a test performed by Method D422 on a duplicate soil sample, provides an indication of the natural dispersive characteristics of clay soils (1).

1.2 This test method is applicable only to soils with a plasticity index greater than 4 as determined in accordance with Method D4318 and more than 12% of the soil fraction finer than 5-[mu]m as determined in accordance with Method D422 (2).

1.3 This test method is similar to Method D422, except that this method covers the determination of percent of soil particles smaller than 5-[mu]m in diameter in a soil-water suspension without mechanical agitation and to which no dispersing agent has been added.

1.4 The amount of particles smaller than 5-[mu]m determined by this method compared with the total amount of particles smaller than 5-[mu]m determined by Method D422 is a measure of the dispersive characteristics of the soil.

1.5 This test method may not identify all dispersive clay soils.

1.6 This standard does not purport to address the safety problems associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

 
2. Referenced Documents

E145-19(2024)

Standard Specification for Gravity-Convection and Forced-Ventilation Ovens

E100-19(2024)

Standard Specification for ASTM Hydrometers

E1-14(2025)

Standard Specification for ASTM Liquid-in-Glass Thermometers

D4318-26

Standard Test Methods for Liquid Limit, Plastic Limit, and Plasticity Index of Soils

E11-24

Standard Specification for Woven Wire Test Sieve Cloth and Test Sieves

D3740-26

Standard Practice for Minimum Requirements for Agencies Engaged in Testing of Soil and Rock as Used in Engineering Design and Construction

D2251-10(2025)

Standard Test Method for Metal Corrosion by Halogenated Organic Solvents and Their Admixtures

D6026-21

Standard Practice for Using Significant Digits and Data Records in Geotechnical Data

D4753-25

Standard Guide for Evaluating, Selecting, and Specifying Balances and Standard Masses for Use in Soil, Rock, and Construction Materials Testing

D422-63(1998)

Standard Test Method for Particle-Size Analysis of Soils

D653-26a

Standard Terminology Relating to Soil, Rock, and Contained Fluids (Includes all amendments and changes 6/15/2026).

D2216-19

Standard Test Methods for Laboratory Determination of Water (Moisture) Content of Soil and Rock by Mass

D4647-06

Standard Test Method for Identification and Classification of Dispersive Clay Soils by the Pinhole Test