ASTM D7545-09 - 1.7.2009
 
Significance and Use

The induction period may be used as an indication of the oxidation and storage stability of middle distillate fuel.

Compared to some other oxidation and storage stability test methods, this method uses a small sample and gives a result in a short time period.

 
1. Scope

1.1 This laboratory test method covers a quantitative determination of the stability of middle distillate fuels such as diesel fuels and heating oils, with up to 100% biodiesel, under accelerated oxidation conditions, by an automatic instrument.

1.2 This test method is designed for products complying with Specification D 975 on Diesel Fuel, Grades No. 1D and 2D; Specification D 396 on Burner Fuel, Grades No. 1 and No. 2; Specification D 6751 on Biodiesel, B100, and Specification D 7467 on Diesel Fuel Oil, B6 to B20.

1.3 This test method measures the induction period, under specified conditions, which can be used as an indication of the oxidation and storage stability of middle distillate fuels.

1.4 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.

1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

 
2. Referenced Documents

D975-26b

Standard Specification for Diesel Fuel (Includes all amendments and changes 3/31/2026).

D4177-22e1

Standard Practice for Automatic Sampling of Petroleum and Petroleum Products (Includes all amendments and changes 3/24/2023).

D6751-24

Standard Specification for Biodiesel Fuel Blendstock (B100) for Middle Distillate Fuels

D7467-23

Standard Specification for Diesel Fuel Oil, Biodiesel Blend (B6 to B20)

CEN/TR 16366:2012

Liquid Petroleum Products--Middle Distillates and Fatty Acid Methyl Ester (FAME) Fuels and Blends--Round Robin Report on Applicability of Rapid Small Scale Oxidation Test Method Available from European Committee for Standardization (CEN), Avenue Marnix 17, B-1000, Brussels, Belgium, http://www.cen.eu.

EN 590

Automotive Fuels--Diesel--Requirements and Test Methods

EN 16091

Liquid Petroleum Products--Middle Distillates and Fatty Acid Methyl Ester (FAME) Fuels and Blends--Determination of Oxidation Stability by Rapid Small Scale Oxidation Method

ISO 4259

Petroleum Products--Determination and Application of Precision Data in Relation to Methods of Test Available from International Organization for Standardization (ISO), 1, ch. de la Voie-Creuse, CP 56, CH-1211 Geneva 20, Switzerland, http://www.iso.org.

D396-26a

Standard Specification for Fuel Oils (Includes all amendments and changes 4/14/2026).

D4057-22

Standard Practice for Manual Sampling of Petroleum and Petroleum Products