ASTM D7889-21 - 1.7.2021
 
Significance and Use

5.1This test method provides a means for obtaining useful in-service fluid analysis properties in the field. It is not to be confused with laboratory or portable FTIR devices which provide measurements per the existing Test Methods listed in 4.1.1.1. Each of these monitored properties has been shown over time to indicate either contamination in the fluid system or a particular breakdown modality of the fluid, which is critical information to assess the health of the fluid as well as the machinery. By utilizing the field device, it is possible for those operating machinery, in locations and situations where it is not practical to gather a sample for the laboratory, to obtain quality in-service fluid analysis. This may be due to the need to have an analysis done in real-time, on-the-spot to maximize the operational hours of equipment, or to have the analysis performed at a location where no laboratory analysis is available.

 
1. Scope

1.1This test method describes the use of a grating spectrometer to analyze properties of an in-service fluid sample which are indicative of the status of that fluid and related machinery.

1.2This test method provides a means for the assessment of in-service fluid properties using infrared spectroscopy. It describes a methodology for sampling, performing analysis, and providing key in-service fluid properties with a self-contained unit that is meant for field use. It provides analysis of in-service fluids at any stage of their useful life, including newly utilized fluid.

1.3In particular, these key in-service fluid properties include oxidation, nitration, sulfation, soot, and antiwear additives. They are applicable for hydrocarbon type (API Group I-IV) fluids from machinery lubricants, including reciprocating engine oils, turbine oils, hydraulic oils, and gear oils.

1.4The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.

1.4.1ExceptionThe unit for wavenumbers is in cm-1.

1.5This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.

1.6This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

 
2. Referenced Documents

D4057-22

Standard Practice for Manual Sampling of Petroleum and Petroleum Products

D7412-22

Standard Test Method for Condition Monitoring of Phosphate Antiwear Additives in In-Service Petroleum and Hydrocarbon Based Lubricants by Trend Analysis Using Fourier Transform Infrared (FT-IR) Spectrometry

D7414-22

Standard Test Method for Condition Monitoring of Oxidation in In-Service Petroleum and Hydrocarbon Based Lubricants by Trend Analysis Using Fourier Transform Infrared (FT-IR) Spectrometry

D7415-22

Standard Test Method for Condition Monitoring of Sulfate By-Products in In-Service Petroleum and Hydrocarbon Based Lubricants by Trend Analysis Using Fourier Transform Infrared (FT-IR) Spectrometry

D7418-23

Standard Practice for Set-Up and Operation of Fourier Transform Infrared (FT-IR) Spectrometers for In-Service Oil Condition Monitoring

D7624-22

Standard Test Method for Condition Monitoring of Nitration in In-Service Petroleum and Hydrocarbon-Based Lubricants by Trend Analysis Using Fourier Transform Infrared (FT-IR) Spectrometry

D7669-20

Standard Guide for Practical Lubricant Condition Data Trend Analysis

D7720-21(2025)

Standard Guide for Statistically Evaluating Measurand Alarm Limits when Using Oil Analysis to Monitor Equipment and Oil for Fitness and Contamination

D7844-22a

Standard Test Method for Condition Monitoring of Soot in In-Service Lubricants by Trend Analysis using Fourier Transform Infrared (FT-IR) Spectrometry (Includes all amendments and changes 10/10/2022).

E131-10(2023)

Standard Terminology Relating to Molecular Spectroscopy

E168-16(2023)

Standard Practices for General Techniques of Infrared Quantitative Analysis

E932-89(2021)

Standard Practice for Describing and Measuring Performance of Dispersive Infrared Spectrometers

E1655-17(2024)

Standard Practices for Infrared Multivariate Quantitative Analysis

E2412-23a

Standard Practice for Condition Monitoring of In-Service Lubricants by Trend Analysis Using Fourier Transform Infrared (FT-IR) Spectrometry (Includes all amendments and changes 11/14/2023).

E2617-17(2024)

Standard Practice for Validation of Empirically Derived Multivariate Calibrations