ASTM D8004-15 - 1.10.2015
 
Significance and Use

5.1 This test method provides a means for a reliable field determination of fuel dilution that is quick and preparation-free. Results are obtained in approximately 1 min. Such a method is used, for example, at remote railroad depots where it is impractical to carry out a standard laboratory method for determination of fuel dilution, such as described in Test Method D7593, but it is a critical need to determine if fuel has contaminated the lubricant. If fuel has contaminated the lubricant, this is significantly detrimental to the machinery and it is typically serviced immediately. Further, the fuel can ignite at the high temperatures encountered in machinery lubricant paths.

 
1. Scope

1.1 This test method describes a means for determining the amount of fuel dilution present in an in-service lubricant. This is achieved by drawing into a surface acoustic wave (SAW) sensor vapor from the lubricant. Fuel vapor will be absorbed by the SAW sensor’s polymer coating. The amount of absorbance is then related to fuel content in the lubricant.

1.2 The range of fuel dilution capable of being measured by the test method is from 0.1 % to 10.0 % by mass fuel dilution.

1.3 This test method is specifically tailored to determining the fuel dilution of in-service lubricants, including newly utilized lubricants. The method is applicable to contamination with diesel, gasoline, and jet fuels.

1.4 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.

1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.See Section 9.

 
2. Referenced Documents

D7720-21(2025)

Standard Guide for Statistically Evaluating Measurand Alarm Limits when Using Oil Analysis to Monitor Equipment and Oil for Fitness and Contamination

D6708-24

Standard Practice for Statistical Assessment and Improvement of Expected Agreement Between Two Test Methods that Purport to Measure the Same Property of a Material

D7235-21a

Standard Guide for Establishing a Linear Correlation Relationship Between Analyzer and Primary Test Method Results Using Relevant ASTM Standard Practices (Includes all amendments and changes 12/21/2021).

D7593-22

Standard Test Method for Determination of Fuel Dilution for In-Service Engine Oils by Gas Chromatography

D7669-20

Standard Guide for Practical Lubricant Condition Data Trend Analysis

E456-13a(2022)e1

Standard Terminology Relating to Quality and Statistics (Includes all amendments and changes 4/16/2024).

D4057-22

Standard Practice for Manual Sampling of Petroleum and Petroleum Products