ASTM E1356-98 - 10.5.1998
 
1. Scope

1.1 This test method covers the determination of the glass transition temperature of materials using differential scanning calorimetry or differential thermal analysis.

1.2 This test method is applicable to amorphous materials or to partially crystalline materials containing amorphous regions, that are stable and do not undergo decomposition or sublimation in the glass transition region.

1.3 The normal operating temperature range is from -120 to 500°C. The temperature range may be extended, depending upon the instrumentation used.

1.4 Computer or electronic-based instruments, techniques, or data treatment equivalent to this test method may also be used. Users of this test method are expressly advised that all such instruments or techniques may not be equivalent. It is the responsibility of the user of this standard to determine the necessary equivalency prior to use. In the case of dispute, only the manual procedures described in this test method are to be considered valid.

1.5 This standard does not purport to address the safety problems associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

 
2. Referenced Documents

E967-18

Standard Test Method for Temperature Calibration of Differential Scanning Calorimeters and Differential Thermal Analyzers

E177-20

Standard Practice for Use of the Terms Precision and Bias in ASTM Test Methods

11357–2

Differential Scanning Calorimetry (DSC)-Part 2 Determination of Glass Transition Temperature

E1142-23b

Standard Terminology Relating to Thermophysical Properties (Includes all amendments and changes 10/5/2023).

E473-23b

Standard Terminology Relating to Thermal Analysis and Rheology (Includes all amendments and changes 10/5/2023).

E691-23

Standard Practice for Conducting an Interlaboratory Study to Determine the Precision of a Test Method