ASTM E1382-97 - 10.4.1997
 
1. Scope

1.1 These test methods are used to determine grain size from measurements of grain intercept lengths, intercept counts, intersection counts, grain boundary length, and grain areas.

1.2 These measurements are made with a semiautomatic digitizing tablet or by automatic image analysis using an image of the grain structure produced by a microscope.

1.3 These test methods are applicable to any type of grain structure or grain size distribution as long as the grain boundaries can be clearly delineated by etching and subsequent image processing, if necessary.

1.4 These test methods are applicable to measurement of other grain-like microstructures, such as cell structures.

1.5 This standard deals only with the recommended test methods and nothing in it should be construed as defining or establishing limits of acceptability or fitness for purpose of the materials tested.

1.6 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

1.7 The sections appear in the following order:

Section Section Scope 1 Referenced Documents 2 Terminology 3 Definitions 3.1 Descriptions of Terms Specific to This Standard 3.2 Symbols 3.3 Summary of Test Method 4 Significance and Use 5 Interferences 6 Apparatus 7 Sampling 8 Test Specimens 9 Specimen Preparation 10 Calibration 11 Procedure: Semiautomatic Digitizing Tablet 12 Intercept Lengths 12.3 Intercept and Intersection Counts 12.4 Grain Counts 12.5 Grain Areas 12.6 ALA Grain Size 12.6.1 Two-Phase Grain Structures 12.7 Procedure: Automatic Image Analysis 13 Grain Boundary Length 13.5 Intersection Counts 13.6 Mean Chord (Intercept) Length/Field 13.7 Individual Chord (Intercept) Lengths 13.7.4 Grain Counts 13.8 Mean Grain Area/Field 13.9 Individual Grain Areas 13.9.4 ALA Grain Size 13.9.8 Two-Phase Grain Structures 13.10 Calculation of Results 14 Test Report 15 Precision and Bias 16 Grain Size of Non-Equiaxed Grain Structure Specimens A1 Examples of Proper and Improper Grain Boundary Delineation A2
 
2. Referenced Documents

E1181-02(2023)

Standard Test Methods for Characterizing Duplex Grain Sizes

E3-11(2017)

Standard Guide for Preparation of Metallographic Specimens

E930-18

Standard Test Methods for Estimating the Largest Grain Observed in a Metallographic Section (ALA Grain Size)

E112-13(2021)

Standard Test Methods for Determining Average Grain Size

E407-23

Standard Practice for Microetching Metals and Alloys

E562-19e1

Standard Test Method for Determining Volume Fraction by Systematic Manual Point Count (Includes all amendments and changes 8/24/2020).

E883-11(2017)

Standard Guide for Reflected-Light Photomicrography

E1245-03(2023)

Standard Practice for Determining the Inclusion or Second-Phase Constituent Content of Metals by Automatic Image Analysis

E7-22

Standard Terminology Relating to Metallography