ASTM E1488-09 - 15.5.2009
 
Significance and Use

All ASTM test methods are required to include statements on precision and bias.

Since ASTM began to require all test methods to have precision and bias statements that are based on interlaboratory test methods, there has been increased concern regarding what statistical experiments and procedures to use during the development of the test methods. Although there exists a wide range of statistical procedures, there is a small group of generally accepted techniques that are very beneficial to follow. This document is designed to provide a brief overview of these procedures and to suggest an appropriate sequence of carrying out these procedures.

Statistical procedures often result in interpretations that are not absolutes. Sometimes the information obtained may be inadequate or incomplete, which may lead to additional questions and the need for further experimentation. Information outside the data is also important in establishing standards and in the interpretation of numerical results.


FIG. 1 Sequence of Steps

 
1. Scope

1.1 This guide identifies statistical procedures for use in developing new test methods or revising or evaluating existing test methods, or both.

1.2 This guide also cites statistical procedures especially useful in the application of test methods.

 
2. Referenced Documents

E2282-23

Standard Guide for Defining the Test Result of a Test Method

E1402-13(2023)

Standard Guide for Sampling Design

E177-20

Standard Practice for Use of the Terms Precision and Bias in ASTM Test Methods

E2554-18e1

Standard Practice for Estimating and Monitoring the Uncertainty of Test Results of a Test Method Using Control Chart Techniques (Includes all amendments and changes 10/7/2019).

E1169-21

Standard Practice for Conducting Ruggedness Tests

E2655-14(2020)

Standard Guide for Reporting Uncertainty of Test Results and Use of the Term Measurement Uncertainty in ASTM Test Methods

E2586-19e1

Standard Practice for Calculating and Using Basic Statistics (Includes all amendments and changes 4/23/2020).

E178-21

Standard Practice for Dealing With Outlying Observations

E456-13a(2022)

Standard Terminology Relating to Quality and Statistics (Includes all amendments and changes 4/21/2022).

E2489-21

Standard Practice for Statistical Analysis of One-Sample and Two-Sample Interlaboratory Proficiency Testing Programs

E691-23

Standard Practice for Conducting an Interlaboratory Study to Determine the Precision of a Test Method

E2587-16(2021)e1

Standard Practice for Use of Control Charts in Statistical Process Control (Includes all amendments and changes 7/28/2021).