ASTM E1568-03 - 10.6.2003
 
Significance and Use

In the primary metallurgical processes used by the mineral processing industry for gold bearing ores, gold is extracted with alkaline cyanide solutions and adsorbed onto activated carbon for recovery of the metal. Metallurgical accounting, process control, and ore evaluation procedures for this type of mineral processing plant depend on accurate, precise, and prompt measurements of gold concentrations in the activated carbon.

This test method for gold in activated carbon is intended primarily as a referee method to test such materials for metal content. It is assumed that those who use these procedures will be trained analysts capable of performing common laboratory procedures skillfully and safely. It is expected that work will be performed in a properly equipped laboratory and that proper waste disposal procedures will be followed. Appropriate quality control practices must be followed, such as those described in Guide E 882.

 
1. Scope

1.1 This test method covers the determination of gold in activated carbon by fire assay collection and gravimetric measurement. It covers the range of 15 to 5000 μg/g gold.

1.2 The values stated in SI units are to be regarded as the standard. The values given in parentheses are for information only.

1.3 This standard does not purport to address all of the safety problems, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. For specific hazards statements, see Section 9 and Notes 2-4, Note 6, and Note 7.

 
2. Referenced Documents

E50-17

Standard Practices for Apparatus, Reagents, and Safety Considerations for Chemical Analysis of Metals, Ores, and Related Materials

E29-22

Standard Practice for Using Significant Digits in Test Data to Determine Conformance with Specifications

D2867-23

Standard Test Methods for Moisture in Activated Carbon

D2866-11(2018)

Standard Test Method for Total Ash Content of Activated Carbon

D2862-16(2022)

Standard Test Method for Particle Size Distribution of Granular Activated Carbon

E276-21

Standard Test Method for Particle Size or Screen Analysis at 4.75 mm (No. 4) Sieve and Finer for Metal-Bearing Ores and Related Materials

E1601-19

Standard Practice for Conducting an Interlaboratory Study to Evaluate the Performance of an Analytical Method

E300-03(2022)

Standard Practice for Sampling Industrial Chemicals

E173-93

Practice for Conducting Interlaboratory Studies of Methods for Chemical Analysis of Metals (Withdrawn 1997)

E882-10(2016)e1

Standard Guide for Accountability and Quality Control in the Chemical Analysis Laboratory (Includes all amendments and changes 10/27/2017).

E135-23a

Standard Terminology Relating to Analytical Chemistry for Metals, Ores, and Related Materials (Includes all amendments and changes 7/17/2023).