ASTM E1613-99 - 10.10.1999
 
1. Scope

1.1 This test method is intended for use with digested samples that were collected originally during the abatement of lead hazards from buildings and related structures.

1.2 This test method covers the lead analysis of sample digestates (for example, digested paint, soil, dust, and airborne particulate) using inductively coupled plasma atomic emission spectrometry (ICP-AES), flame atomic absorption spectrometry (FAAS), and graphite furnace atomic absorption spectrometry (GFAAS) techniques.

1.3 No detailed operating instructions can be provided because of differences among various makes and models of satisfactory instruments. Instead, the analyst should follow the instructions provided by the manufacturer of the particular instrument.

1.4 This test method contains directions for sample analysis as well as quality assurance (QA) and quality control (QC) and may be used for purposes of laboratory accreditation and certification.

1.5 The use of analytical instrumentation other than ICP-AES, FAAS, and GFAAS is not within the scope of this test method.

1.6 The values stated in SI units are to be regarded as the standard.

1.7 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

 
2. Referenced Documents

E1605-22

Standard Terminology Relating to Lead in Buildings

E1644-21

Standard Practice for Hot Plate Digestion of Dust Wipe Samples for the Determination of Lead

E1645-21

Standard Practice for Preparation of Dried Paint Samples by Hotplate or Microwave Digestion for Subsequent Lead Analysis

D1193-06(2018)

Standard Specification for Reagent Water

D3919-15

Standard Practice for Measuring Trace Elements in Water by Graphite Furnace Atomic Absorption Spectrophotometry

D4210-89(1996)e1

Standard Practice for Intralaboratory Quality Control Procedures and a Discussion on Reporting Low-Level Data (Withdrawn 2002)

D4697-95(2001)

Standard Guide for Maintaining Test Methods in the User's Laboratory (Withdrawn 2009)

D4840-99(2018)e1

Standard Guide for Sample Chain-of-Custody Procedures (Includes all amendments and changes 8/22/2018).

D6785-20

Standard Test Method for Determination of Lead in Workplace Air Using Flame or Graphite Furnace Atomic Absorption Spectrometry

D7144-21

Standard Practice for Collection of Surface Dust by Micro-vacuum Sampling for Subsequent Determination of Metals and Metalloids

E456-13a(2022)

Standard Terminology Relating to Quality and Statistics (Includes all amendments and changes 4/21/2022).

E691-23

Standard Practice for Conducting an Interlaboratory Study to Determine the Precision of a Test Method

E1188-23

Standard Practice for Collection and Preservation of Information and Physical Items by a Technical Investigator

E1726-21

Standard Practice for Preparation of Soil Samples by Hotplate Digestion for Subsequent Lead Analysis

E1727-20

Standard Practice for Field Collection of Soil Samples for Subsequent Lead Determination

E1728-16

Standard Practice for Collection of Settled Dust Samples Using Wipe Sampling Methods for Subsequent Lead Determination

E1729-20

Standard Practice for Field Collection of Dried Paint Samples for Subsequent Lead Determination

E1741-00

Standard Practice for Preparation of Airborne Particulate Lead Samples Collected During Abatement and Construction Activities for Subsequent Analysis by Atomic Spectrometry (Withdrawn 2009)

E1775-20

Standard Guide for Evaluating Performance of On-Site Extraction and Field-Portable Electrochemical or Spectrophotometric Analysis for Lead

E1792-20

Standard Specification for Wipe Sampling Materials for Lead in Surface Dust

E1864-02

Standard Practice for Evaluating Quality Systems of Organizations Conducting Facility and Hazard Assessments for Lead in Paint, Dust, Airborne Particulate, and Soil in and around Buildings and Related Structures (Withdrawn 2011)

E1979-21

Standard Practice for Ultrasonic Extraction of Paint, Dust, Soil, and Air Samples for Subsequent Determination of Lead

E2239-20

Standard Practice for Record Keeping and Record Preservation for Lead Hazard Activities