ASTM E1747-95 - 1.1.1995
 
1. Scope

1.1 This guide defines purity standards for carbon dioxide to ensure the suitability of liquefied carbon dioxide gas for use in SFE and SFC applications (see Guide E1449 for definitions of terms). This guide defines quantitation, labeling, and statistical standards for impurities in carbon dioxide that are necessary for successful SFE or SFC laboratory work, and it suggests methods of analysis for quantifying these impurities.

1.2 This guide is provided for use by specialty gas suppliers who manufacture carbon dioxide specifically for SFE or SFC applications. SFE or SFC CO 2 products offered with a claim of adherence to this guide will meet certain absolute purity and contaminant detectability requirements matched to the needs of current SFE or SFC techniques. The use of this guide allows different SFE or SFC CO 2 product offerings to be compared on an equal purity basis.

1.3 This guide considers contaminants to be those components that either cause detector signals that interfere with those of the target analytes or physically impede the SFE or SFC experiment.

1.4 The values stated in SI units are to be regarded as the standard.

1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

 
2. Referenced Documents

D3670-91(2022)

Standard Guide for Determination of Precision and Bias of Methods of Committee D22

D2820-72(1978)

Test Method for C through C Hydrocarbons in the Atmosphere by Gas Chromatography (Withdrawn 1993)

D2504-88(1998)

Standard Test Method for Noncondensable Gases in C2 and Lighter Hydrocarbon Products by Gas Chromatography

D3687-19

Standard Test Method for Analysis of Organic Compound Vapors Collected by the Activated Charcoal Tube Adsorption Method

D3686-20

Standard Practice for Sampling Atmospheres to Collect Organic Compound Vapors (Activated Charcoal Tube Adsorption Method)

E1510-95(2021)

Standard Practice for Installing Fused Silica Open Tubular Capillary Columns in Gas Chromatographs

D4532-22

Standard Test Method for Respirable Dust in Workplace Atmospheres Using Cyclone Samplers

D4178-23

Standard Practice for Calibrating Moisture Analyzers

E260-96(2019)

Standard Practice for Packed Column Gas Chromatography

E1449-92(2019)

Standard Guide for Supercritical Fluid Chromatography Terms and Relationships

E697-96(2019)

Standard Practice for Use of Electron-Capture Detectors in Gas Chromatography

E594-96(2019)

Standard Practice for Testing Flame Ionization Detectors Used in Gas or Supercritical Fluid Chromatography

E355-96(2021)e1

Standard Practice for Gas Chromatography Terms and Relationships (Includes all amendments and changes 4/28/2021).