ASTM E2113-09 - 1.9.2009
 
Significance and Use

Performance verification or calibration is essential to the accurate determination of quantitative dimension change measurements.

This test method may be used for instrument performance validation, regulatory compliance, research and development and quality assurance purposes.

 
1. Scope

1.1 This test method describes calibration of the length change (deflection) measurement or thermal expansion of thermomechanical analyzers (TMA) within the temperature range from -150 to 1000 °C using the thermal expansion of a suitable reference material.

1.2 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.

1.3 This test method differs from ISO standard 11359-1 by providing an alternative calibration procedure.

1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of whoever uses this standard to consult and establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

 
2. Referenced Documents

E2161-23c

Standard Terminology Relating to Performance Validation in Thermal Analysis and Rheology (Includes all amendments and changes 8/17/2023).

E1363-23

Standard Test Method for Temperature Calibration of Thermomechanical Analyzers

E1142-23b

Standard Terminology Relating to Thermophysical Properties (Includes all amendments and changes 10/5/2023).

E831-19

Standard Test Method for Linear Thermal Expansion of Solid Materials by Thermomechanical Analysis

E473-23b

Standard Terminology Relating to Thermal Analysis and Rheology (Includes all amendments and changes 10/5/2023).

ISO?11359-1

Plastics--Thermomechanical analysis (TMA)--Part 1: General principles Available from American National Standards Institute (ANSI), 25 W. 43rd St., 4th Floor, New York, NY 10036, http://www.ansi.org.