ASTM E2294-03(2013) - 1.11.2013
 
Significance and Use

5.1 This practice is primarily intended to be used for the correction of silver loss in the fire assay process. Silver assays are determined by fire assay for the purpose of metallurgical exchange between seller and buyer.

5.2 It is assumed that all who use this practice will be trained analysts capable of performing skillfully and safely. It is expected that work will be performed in a properly equipped laboratory under appropriate quality control practices such as those described in Guide E882.

 
1. Scope

1.1 This practice covers the determination of fire assay correction for silver, utilizing proof silver, ores, concentrates, and related metallurgical materials.

1.2 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.

1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. (See Test Methods E1335, Practices E50, Guide E882, and ISO Guide 35: 1989.)

 
2. Referenced Documents

E50-17

Standard Practices for Apparatus, Reagents, and Safety Considerations for Chemical Analysis of Metals, Ores, and Related Materials

E882-10(2016)e1

Standard Guide for Accountability and Quality Control in the Chemical Analysis Laboratory (Includes all amendments and changes 10/27/2017).

E29-22

Standard Practice for Using Significant Digits in Test Data to Determine Conformance with Specifications

ISO?Guide?35:?1989

Certification of Reference Materials- General and Statistical Principles

E135-23a

Standard Terminology Relating to Analytical Chemistry for Metals, Ores, and Related Materials (Includes all amendments and changes 7/17/2023).

ISO?10378:?1994

Copper Sulfide Concentrates-Determination of Gold and Silver Contents-Fire Assay Gravimetric and Atomic Absorption Spectrometric Method

E1335-08(2017)

Standard Test Methods for Determination of Gold in Bullion by Fire Assay Cupellation Analysis