ASTM E2716-09(2014) - 15.3.2014
 
Significance and Use

5.1 Modulated temperature differential scanning calorimetric measurements provide a rapid, simple method for determining specific heat capacities of materials, even under quasi-isothermal conditions.

5.2 Specific heat capacities are important for design purposes, quality control, and research and development.

5.3 The use of a stepped quasi-isothermal program may be used to follow structure changes in materials.

 
1. Scope

1.1 This test method describes the determination of specific heat capacity by sinusoidal modulated temperature differential scanning calorimetry. For the determination of specific heat capacity by a step-isothermal or multiple step-isothermal temperature program, the reader is referred to Test Method E1269.

1.2 This test method is generally applicable to thermally stable solids and liquids.

1.3 The normal operating range of the test is from –100 to 600°C. The temperature range may be extended depending upon the instrumentation and specimen holders used.

1.4 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.

1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

 
2. Referenced Documents

E1269-11(2018)

Standard Test Method for Determining Specific Heat Capacity by Differential Scanning Calorimetry

E1142-23b

Standard Terminology Relating to Thermophysical Properties (Includes all amendments and changes 10/5/2023).

E968-02

Standard Practice for Heat Flow Calibration of Differential Scanning Calorimeters

E967-18

Standard Test Method for Temperature Calibration of Differential Scanning Calorimeters and Differential Thermal Analyzers

E473-23b

Standard Terminology Relating to Thermal Analysis and Rheology (Includes all amendments and changes 10/5/2023).