ASTM E315-04 - 1.5.2004
 
Significance and Use

These test methods for the chemical analysis of metals and alloys are primarily intended to test such materials for compliance with compositional specifications. It is assumed that all who use these test methods will be trained analysts capable of performing common laboratory procedures skillfully and safely. It is expected that work will be performed in a properly equipped laboratory.

 
1. Scope

1.1 These test methods cover the chemical analysis of molybdenum and molybdenum alloys having chemical compositions within the following limits:
ElementConcentration Range, %
Carbon0.010 to 0.040
Iron0.020 max
Molybdenum99.25 to 99.99
Nickel0.010 max
Nitrogen0.0010 max
Oxygen0.0030 max
Silicon0.010 max
Titanium0.005 to 0.55
Zirconium0.06 to 0.12

1.2 The test methods in this standard are contained in the sections indicated below:

Sections
Nickel by the Persulfate-Dimethylglyoxime Photometric Method9-18
Iron by the 1,10-Phenanthroline Photometric Method19-29
Silicon by the Molybdenum Blue-Extraction Photometric Method30-40

1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. Specific precautionary information is given in Section 5.

 
2. Referenced Documents

E50-17

Standard Practices for Apparatus, Reagents, and Safety Considerations for Chemical Analysis of Metals, Ores, and Related Materials

E60-11(2022)e1

Standard Practice for Analysis of Metals, Ores, and Related Materials by Spectrophotometry (Includes all amendments and changes 6/29/2022).

E1601-19

Standard Practice for Conducting an Interlaboratory Study to Evaluate the Performance of an Analytical Method

E29-22

Standard Practice for Using Significant Digits in Test Data to Determine Conformance with Specifications

E173-93

Practice for Conducting Interlaboratory Studies of Methods for Chemical Analysis of Metals (Withdrawn 1997)

B386-03

Standard Specification for Molybdenum and Molybdenum Alloy Plate, Sheet, Strip, and Foil

B385-74

Specification for Molybdenum and Molybdenum Alloy Billets for Reforging (Withdrawn 1985)

B384-74

Specification for Molybdenum and Molybdenum Alloy Forgings (Withdrawn 1984)

B387-18

Standard Specification for Molybdenum and Molybdenum Alloy Bar, Rod, and Wire