ASTM E352-93(2006) - 1.6.2006
 
Significance and Use

These test methods for the chemical analysis of metals and alloys are primarily intended as referee methods to test such materials for compliance with compositional specifications particularly those under the jurisdiction of ASTM Committee A1 on Steel, Stainless Steel, and Related Alloys. It is assumed that all who use these test methods will be trained analysts capable of performing common laboratory procedures skillfully and safely. It is expected that work will be performed in a properly equipped laboratory under appropriate quality control practices such as those described in Guide E 882.

 
1. Scope

1.1 These test methods cover the chemical analysis of tool steels and other similar medium- and high-alloy steels having chemical compositions within the following limits:

1.3 Test methods for the determination of several elements not included in this standard can be found in Test Methods E 30 and Test Methods E 1019.

1.4 Some of the concentration ranges given in are too broad to be covered by a single test method and therefore this standard contains multiple test methods for some elements. The user must select the proper test method by matching the information given in the Scope and Interference sections of each test method with the composition of the alloy to be analyzed.

1.5 The values stated in SI units are to be regarded as standard. In some cases, exceptions allowed in Practice E 380 are also used.

This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. Specific hazards statements are given in Section and in special "Warning" paragraphs throughout these test methods.

1.6 This method covers the determination of manganese in concentrations from 0.10 to 5.00 %.

1.7 This test method covers the determination of phosphorus in concentrations from 0.002 to 0.05 %.

 
2. Referenced Documents

E173-93

Practice for Conducting Interlaboratory Studies of Methods for Chemical Analysis of Metals (Withdrawn 1997)

D1193-06(2018)

Standard Specification for Reagent Water

E29-22

Standard Practice for Using Significant Digits in Test Data to Determine Conformance with Specifications

E50-17

Standard Practices for Apparatus, Reagents, and Safety Considerations for Chemical Analysis of Metals, Ores, and Related Materials

E60-11(2022)e1

Standard Practice for Analysis of Metals, Ores, and Related Materials by Spectrophotometry (Includes all amendments and changes 6/29/2022).

E135-23a

Standard Terminology Relating to Analytical Chemistry for Metals, Ores, and Related Materials (Includes all amendments and changes 7/17/2023).

ISO 5725

Precision of Test Methods--Determination of Repeatability and Reproducibility for Inter-Laboratory Tests

E351-18

Standard Test Methods for Chemical Analysis of Cast IronĀ“All Types

E353-19e1

Standard Test Methods for Chemical Analysis of Stainless, Heat-Resisting, Maraging, and Other Similar Chromium-Nickel-Iron Alloys (Includes all amendments and changes 2/23/2022).

E882-10(2016)e1

Standard Guide for Accountability and Quality Control in the Chemical Analysis Laboratory (Includes all amendments and changes 10/27/2017).

E1019-18

Standard Test Methods for Determination of Carbon, Sulfur, Nitrogen, and Oxygen in Steel, Iron, Nickel, and Cobalt Alloys by Various Combustion and Inert Gas Fusion Techniques

E1024-97

Standard Guide for Chemical Analysis of Metals and Metal Bearing Ores by Flame Atomic Absorption Spectrophotometry

E1806-23

Standard Practice for Sampling Steel and Iron for Determination of Chemical Composition

E350-23

Standard Test Methods for Chemical Analysis of Carbon Steel, Low-Alloy Steel, Silicon Electrical Steel, Ingot Iron, and Wrought Iron