ASTM F3181-16 - 1.2.2016
 
Significance and Use

4.1 This test method is a way to evaluate the effects of contaminant particles found in HDPE products containing PCR-HDPE, primarily corrugated pipe. Particles of significant number, size and shape can reduce the slow crack growth resistance of the products. This test is performed in water without a controlled defect such as a notch. Since there is no notch, it is not necessary to use a surfactant in the water bath. It is a constant load test.

4.2 This test may be used to evaluate various blends of recycled and virgin materials. For example, a material with high stress crack resistance and few contaminants can be blended with materials that are less resistant to cracking to enhance the overall stress crack resistance of the blend.

4.3 The test can be conducted at various temperature and stress conditions. If at least three (3) different temperature/stress conditions are evaluated, an estimate of the service lifetime of the material can be predicted with the use of bi-directional shifting or the rate process method.

4.4 The test can also be performed under a single applied load and a single temperature to create a single point test useful for comparative purposes as well as for quality control.

 
1. Scope

1.1 This test method covers an un-notched constant ligament stress (UCLS) test for use with HDPE materials that contain post-consumer recycled HDPE (PCR-HDPE). Contaminants in the PCR-HDPE can initiate stress cracks at elevated temperatures, and this test method evaluates the response of these materials to a constant applied stress.

1.2 The test method is focused on HDPE corrugated pipe containing PCR-HDPE, but can be used in other applications where PCR-HDPE is used.

1.3 The test utilizes the same devices used to perform the NCTL test (Test Method D5397) and the NCLS test (Test Method F2136), but the test is conducted with different specimens and with the use of water instead of a surfactant solution. The test specimen is larger than standard NCLS and NCTL specimens to increase the number of contaminant particles in the specimen that might grow cracks.

1.4 The values stated in inch-pound units are to be regarded as standard. The values given in parentheses are mathematical conversions to SI units that are provided for information only and are not considered standard.

1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

 
2. Referenced Documents

D1600-18

Standard Terminology for Abbreviated Terms Relating to Plastics (Withdrawn 2024)

D2837-22

Standard Test Method for Obtaining Hydrostatic Design Basis for Thermoplastic Pipe Materials or Pressure Design Basis for Thermoplastic Pipe Products

D638-22

Standard Test Method for Tensile Properties of Plastics

F412-23

Standard Terminology Relating to Plastic Piping Systems

F2136-18(2024)

Standard Test Method for Notched, Constant Ligament-Stress (NCLS) Test to Determine Slow-Crack-Growth Resistance of HDPE Resins or HDPE Corrugated Pipe

Report 696

National Cooperative Highway Research Program (NCHRP)

D4703-16

Standard Practice for Compression Molding Thermoplastic Materials into Test Specimens, Plaques, or Sheets

D5397-20

Standard Test Method for Evaluation of Stress Crack Resistance of Polyolefin Geomembranes Using Notched Constant Tensile Load Test