ASTM F331-13 - 1.6.2013
 
1. Scope

1.1 This test method covers the determination of nonvolatile matter, that is, residue on evaporation, in solvent extract from aerospace components, using a rotary flash evaporator.

1.2 The procedure for extraction from components is described in practices such as Practice F303. Before subjecting the extract to the following method, it should be processed to remove the insoluble particulate in accordance with Practice F311 (Note 1). Particle count analysis of the removed particulate may then be performed in accordance with Test Method F312. If particulate is not removed from the extract prior to performing this method, this should be noted on the test report.

Note 1Membrane filters with a maximum extractable content of 0.5 weight % should be used on samples to be processed by this test method. Conventional membranes contain 5 to 10 % extractables. For obtaining very low background levels, consideration should be given to using membranes without grid marks.

1.3 The values stated in SI units are to be regarded as standard.

1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

 
2. Referenced Documents

F311-08(2020)

Standard Practice for Processing Aerospace Liquid Samples for Particulate Contamination Analysis Using Membrane Filters

F303-08(2023)e1

Standard Practices for Sampling for Particles in Aerospace Fluids and Components (Includes all amendments and changes 9/20/2023).

F312-08(2023)

Standard Test Methods for Microscopical Sizing and Counting Particles from Aerospace Fluids on Membrane Filters

D1193-06(2018)

Standard Specification for Reagent Water

IEST-STD-1246D

Product Cleanliness Levels and Contamination Control Program